Replication data for: "Comparative study of lattice parameter and pore size of ordered mesoporous silica materials using physisorption, SAXS measurements and transmission electron microscopy"

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Beurer, Ann-Katrin; Dieterich, Sonja; Solodenko, Helena; Kaya, Elif; Merdanoǧlu, Naǧme; Schmitz, Guido; Traa, Yvonne; Bruckner, Johanna R., 2023, "Replication data for: "Comparative study of lattice parameter and pore size of ordered mesoporous silica materials using physisorption, SAXS measurements and transmission electron microscopy"", https://doi.org/10.18419/DARUS-3348, DaRUS, V1

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Description	All primary data files of measurements and processed data of the journal article "Comparative study of lattice parameter and pore size of ordered mesoporous silica materials using physisorption, SAXS measurements and transmission electron microscopy", are deposited. File types which are not easily readable have been converted to other formats, i.e. TIF and TXT, and have been deposited additionally. PDH files may be opened with the same applications as TXT files. The dataset contains the following data: nitrogen physisorption measurements, small-angle X-ray scattering curves, transmission electron micrographs. The data is named according to the sample name. A short description of the samples is given in the following: OMS_TLCT: Ordered mesoporous silica material synthesized via true liquid crystal templating with hexadecylethyldimethylammonium chloride as surfactant MCM-41: Ordered mesoporous silica material synthesized via a cooperative self-assembly process with hexadecyltrimethylammonium chloride as surfactant SBA-15: Ordered mesoporous silica material synthesized via a cooperative self-assembly process with the poloxamer P123 as surfactant SBA-15_sa: Ordered mesoporous silica material synthesized via a cooperative self-assembly process with the poloxamer P123 as surfactant and n-decane as swelling agent (2023)
Subject	Chemistry
Keyword	Mesoporous Silica, MCM-41, Physisorption, Small-Angle X-Ray Scattering (SAXS), Transmission Electron Microscopy (TEM)
Related Publication	Ann-Katrin Beurer, Sonja Dieterich, Helena Solodenko, Elif Kaya, Naǧme Merdanoǧlu, Guido Schmitz, Yvonne Traa, Johanna R. Bruckner, "Comparative study of lattice parameter and pore size of ordered mesoporous silica materials using physisorption, SAXS measurements and transmission electron microscopy", Microporous and Mesoporous Materials, Volume 354, 15 April 2023, 112508.doi: 10.1016/j.micromeso.2023.112508
Data Generation	Experiment
License/Data Use Agreement	CC BY 4.0

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	MCM-41_N2_M1_analysis-adsorption-branch.txt Physisorption measurements/Plain Text - 42.7 KB Published Apr 26, 2023 31 Downloads MD5: 0b5aca408b7ea831a458b6ad3695bec8	Preview "Physisorption measurements/MCM-41_N2_M1_analysis-adsorption-branch.txt" Access File File Access Public Download Options Plain Text Download Metadata Data File Citation EndNote XML RIS BibTeX
	MCM-41_N2_M1_analysis-desorption-branch.txt Physisorption measurements/Plain Text - 42.6 KB Published Apr 26, 2023 37 Downloads MD5: a32c71d97b54aa499ea8f0f4e21dc442	Preview "Physisorption measurements/MCM-41_N2_M1_analysis-desorption-branch.txt" Access File File Access Public Download Options Plain Text Download Metadata Data File Citation EndNote XML RIS BibTeX
	MCM-41_N2_M1_raw-data.qps Physisorption measurements/application/vnd.publishare-delta-tree - 28.4 KB Published Apr 26, 2023 18 Downloads MD5: ec61b9ced4a01dfd2728bdd417056832	Access File File Access Public Download Options application/vnd.publishare-delta-tree Download Metadata Data File Citation EndNote XML RIS BibTeX
	MCM-41_N2_M2_analysis-adsorption-branch.txt Physisorption measurements/Plain Text - 42.7 KB Published Apr 26, 2023 45 Downloads MD5: 8920a0ec2de0e2c6de79427a67bc8193	Preview "Physisorption measurements/MCM-41_N2_M2_analysis-adsorption-branch.txt" Access File File Access Public Download Options Plain Text Download Metadata Data File Citation EndNote XML RIS BibTeX
	MCM-41_N2_M2_analysis-desorption-branch.txt Physisorption measurements/Plain Text - 43.5 KB Published Apr 26, 2023 33 Downloads MD5: d9cc5b8d6554d8c65d06207611e20164	Preview "Physisorption measurements/MCM-41_N2_M2_analysis-desorption-branch.txt" Access File File Access Public Download Options Plain Text Download Metadata Data File Citation EndNote XML RIS BibTeX
	MCM-41_N2_M2_raw-data.RAW Physisorption measurements/Unknown - 6.0 KB Published Apr 26, 2023 17 Downloads MD5: 9f7da4a208ae0f222701587489525e28	Access File File Access Public Download Options Original File Format Download Metadata Data File Citation EndNote XML RIS BibTeX
	OMS_TLCT_N2_M1_analysis-adsorption-branch.txt Physisorption measurements/Plain Text - 45.4 KB Published Apr 26, 2023 38 Downloads MD5: 0195cf48bc8abe4ff1163bc6874d7aea	Preview "Physisorption measurements/OMS_TLCT_N2_M1_analysis-adsorption-branch.txt" Access File File Access Public Download Options Plain Text Download Metadata Data File Citation EndNote XML RIS BibTeX
	OMS_TLCT_N2_M1_analysis-desorption-branch.txt Physisorption measurements/Plain Text - 45.2 KB Published Apr 26, 2023 35 Downloads MD5: 78995372bda595b3414010b2a7518cbc	Preview "Physisorption measurements/OMS_TLCT_N2_M1_analysis-desorption-branch.txt" Access File File Access Public Download Options Plain Text Download Metadata Data File Citation EndNote XML RIS BibTeX
	OMS_TLCT_N2_M1_raw-data.qps Physisorption measurements/application/vnd.publishare-delta-tree - 28.4 KB Published Apr 26, 2023 13 Downloads MD5: 02132a2f4dd1973a3284ef8bf3be78fd	Access File File Access Public Download Options application/vnd.publishare-delta-tree Download Metadata Data File Citation EndNote XML RIS BibTeX
	OMS_TLCT_N2_M2_analysis-adsorption-branch.txt Physisorption measurements/Plain Text - 46.0 KB Published Apr 26, 2023 31 Downloads MD5: 2105ea868dfaba820b92164ff06c8f4c	Preview "Physisorption measurements/OMS_TLCT_N2_M2_analysis-adsorption-branch.txt" Access File File Access Public Download Options Plain Text Download Metadata Data File Citation EndNote XML RIS BibTeX

Citation Metadata

Persistent Identifier	doi:10.18419/DARUS-3348
Publication Date	2023-04-26
Title	Replication data for: "Comparative study of lattice parameter and pore size of ordered mesoporous silica materials using physisorption, SAXS measurements and transmission electron microscopy"
Author	Beurer, Ann-KatrinInstitute of Technical Chemistry, University of Stuttgart Institute of Physical Chemistry, University of Stuttgart1135748381 Institute for Materials Science, University of Stuttgart0000-0002-0306-9412 Institute of Technical Chemistry, University of Stuttgart0009-0006-5909-7347 Institute of Technical Chemistry, University of Stuttgart0009-0008-6224-8219 Institute for Materials Science, University of Stuttgart0000-0002-3642-1195 Institute of Technical Chemistry, University of Stuttgart0000-0001-7393-4291 Institute of Physical Chemistry, University of Stuttgart0000-0001-7183-6532
Point of Contact	Use email button above to contact. Bruckner, Johanna R. (Institute of Physical Chemistry, University of Stuttgart) Traa, Yvonne (Institute of Technical Chemistry, University of Stuttgart)
Description	All primary data files of measurements and processed data of the journal article "Comparative study of lattice parameter and pore size of ordered mesoporous silica materials using physisorption, SAXS measurements and transmission electron microscopy", are deposited. File types which are not easily readable have been converted to other formats, i.e. TIF and TXT, and have been deposited additionally. PDH files may be opened with the same applications as TXT files. The dataset contains the following data: nitrogen physisorption measurements, small-angle X-ray scattering curves, transmission electron micrographs. The data is named according to the sample name. A short description of the samples is given in the following: OMS_TLCT: Ordered mesoporous silica material synthesized via true liquid crystal templating with hexadecylethyldimethylammonium chloride as surfactant MCM-41: Ordered mesoporous silica material synthesized via a cooperative self-assembly process with hexadecyltrimethylammonium chloride as surfactant SBA-15: Ordered mesoporous silica material synthesized via a cooperative self-assembly process with the poloxamer P123 as surfactant SBA-15_sa: Ordered mesoporous silica material synthesized via a cooperative self-assembly process with the poloxamer P123 as surfactant and n-decane as swelling agent (2023)
Subject	Chemistry
Keyword	Mesoporous Silica https://www.wikidata.org/wiki/Q17156473 (Wikidata) MCM-41 https://www.wikidata.org/wiki/Q11231266 (Wikidata) Physisorption http://purl.obolibrary.org/obo/REX_0000207 (REX) Small-Angle X-Ray Scattering (SAXS) https://purl.org/tema/023572 (TEMA) Transmission Electron Microscopy (TEM) http://purl.obolibrary.org/obo/NCIT_C18216 (NCIT)
Topic Classification	Physical Chemistry (NCIT) http://purl.obolibrary.org/obo/NCIT_C16421 Technical Chemistry (LCSH) http://id.loc.gov/authorities/subjects/sh85023029 Material Science (TEMA) https://purl.org/tema/604684
Related Publication	Ann-Katrin Beurer, Sonja Dieterich, Helena Solodenko, Elif Kaya, Naǧme Merdanoǧlu, Guido Schmitz, Yvonne Traa, Johanna R. Bruckner, "Comparative study of lattice parameter and pore size of ordered mesoporous silica materials using physisorption, SAXS measurements and transmission electron microscopy", Microporous and Mesoporous Materials, Volume 354, 15 April 2023, 112508. doi 10.1016/j.micromeso.2023.112508 https://doi.org/10.1016/j.micromeso.2023.112508
Language	English
Project	Project A4 (Level 0) Project C3 (Level 1)
Funding Information	DFG: 358283783 - SFB 1333 Ministry Of Science, Research and the Arts Baden-Württemberg: Margarete von Wrangell program
Depositor	Bruckner, Johanna R.
Deposit Date	2023
Data Type	experimental data

Process Metadata

Processing Methods	SAXS data (Small-angle X-ray scattering (SAXS) data was measured with a slit collimated X-ray beam. The original measurement data is deposited together with the deconvoluted data wich was processed to to eliminate the influcence of the slit collimated beam. Furthermore, cholesteryl palmitate was used to calibrate the sample to detector distance.)
Instruments	SAXSess mc2, Anton Paar , Location: Institute of Physical Chemistry, University of Stuttgart, 70550, Stuttgart, Germany Autosorb iQ, Quantachrome Instruments , Location: Institute of Technical Chemistry, University of Stuttgart, 70550, Stuttgart, Germany FEG CM200, Phillips , Location: Institute for Materials Science, University of Stuttgart, 70550, Stuttgart, Germany

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