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Part 1: Document Description
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Citation |
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Title: |
Replication Data for: "A flavin-inspired covalent organic framework for photocatalytic alcohol oxidation" |
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Identification Number: |
doi:10.18419/darus-2244 |
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Distributor: |
DaRUS |
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Date of Distribution: |
2023-07-18 |
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Version: |
1 |
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Bibliographic Citation: |
Trenker, Stefan; Grunenberg, Lars; Banerjee, Tanmay; Savasci, Gökcen; Poller, Laura M.; Muggli, Katharina I. M.; Haase, Frederik; Ochsenfeld, Christian; Lotsch, Bettina, 2023, "Replication Data for: "A flavin-inspired covalent organic framework for photocatalytic alcohol oxidation"", https://doi.org/10.18419/darus-2244, DaRUS, V1 |
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Citation |
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Title: |
Replication Data for: "A flavin-inspired covalent organic framework for photocatalytic alcohol oxidation" |
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Identification Number: |
doi:10.18419/darus-2244 |
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Authoring Entity: |
Trenker, Stefan (Max Planck Institute for Solid State Research) |
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Grunenberg, Lars (Max Planck Institute for Solid State Research) |
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Banerjee, Tanmay (Birla Institute of Technology and Science Pilani) |
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Savasci, Gökcen (University of Munich (LMU)) |
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Poller, Laura M. (University of Munich (LMU)) |
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Muggli, Katharina I. M. (University of Munich (LMU)) |
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Haase, Frederik (Karlsruhe Institute of Technology (KIT)) |
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Ochsenfeld, Christian (University of Munich (LMU)) |
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Lotsch, Bettina (Max Planck Institute for Solid State Research) |
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Grant Number: |
358283783 - SFB 1333 |
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Grant Number: |
EXC2089 |
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Grant Number: |
info:eu-repo/grantAgreement/EC/H2020/639233 |
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Distributor: |
DaRUS |
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Access Authority: |
Lotsch, Bettina |
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Depositor: |
Trenker, Stefan |
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Date of Deposit: |
2021-11-25 |
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Holdings Information: |
https://doi.org/10.18419/darus-2244 |
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Study Scope |
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Keywords: |
Chemistry, Covalent Organic Framework, Photocatalysis |
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Abstract: |
Covalent organic frameworks (COFs) offer a number of key properties that predestine them to be used as heterogeneous photocatalysts, including intrinsic porosity, long-range order, and light absorption. Since COFs can be constructed from a practically unlimited library of organic building blocks, these properties can be precisely tuned by choosing suitable linkers. Herein, we report the construction and use of a novel COF (FEAx-COF) photocatalyst, inspired by natural flavin cofactors. We show that the functionality of the alloxazine chromophore incorporated into the COF backbone is retained and study the effects of this heterogenization approach by comparison with similar molecular photocatalysts. We find that the integration of alloxazine chromophores into the framework significantly extends the absorption spectrum into the visible range, allowing for photocatalytic oxidation of benzylic alcohols to aldehydes even with low-energy visible light. In addition, the activity of the heterogeneous COF photocatalyst is less dependent on the chosen solvent, making it more versatile compared to molecular alloxazines. Finally, the use of oxygen as the terminal oxidant renders FEAx-COF a promising and “green” heterogeneous photocatalyst. <br> All primary data files of measurements and processed data of the journal article mentioned under related publications from Lotsch group can be found here. The dataset contains data for the following analytical techniques: SEM, TEM, XPRD, scXRD, NMR, IR, UV-Vis, Sorption. |
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Kind of Data: |
experimental data |
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Methodology and Processing |
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Sources Statement |
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Data Access |
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Other Study Description Materials |
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Related Studies |
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Related data has been deposited in the <a href="https://www.ccdc.cam.ac.uk/">Cambridge Crystallographic Data Centre (CCDC)</a><br/> PEAx: Stefan Trenker, Lars Grunenberg, Tanmay Banerjee, Gökcen Savasci, Laura M. Poller, Katharina I. M. Muggli, Frederik Haase, Christian Ochsenfeld, Bettina V. Lotsch CCDC 2097444: Experimental Crystal Structure Determination, 2021, DOI: <a href="https://doi.org/10.5517/ccdc.csd.cc28dkhr">10.5517/ccdc.csd.cc28dkhr</a> |
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<br/> HEAx: Stefan Trenker, Lars Grunenberg, Tanmay Banerjee, Gökcen Savasci, Laura M. Poller, Katharina I. M. Muggli, Frederik Haase, Christian Ochsenfeld, Bettina V. Lotsch CCDC 2097424: Experimental Crystal Structure Determination, 2021, DOI: <a href="https://doi.org/10.5517/ccdc.csd.cc28djv2">10.5517/ccdc.csd.cc28djv2</a> |
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Related Publications |
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Citation |
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Title: |
Stefan Trenker, Lars Grunenberg, Tanmay Banerjee, Gökcen Savasci, Laura M. Poller, Katharina I. M. Muggli, Frederik Haase, Christian Ochsenfeld and Bettina V. Lotsch. A flavin-inspired covalent organic framework for photocatalytic alcohol oxidation. Chem. Sci., 2021,12, 15143-15150. |
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Identification Number: |
10.1039/D1SC04143F |
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Bibliographic Citation: |
Stefan Trenker, Lars Grunenberg, Tanmay Banerjee, Gökcen Savasci, Laura M. Poller, Katharina I. M. Muggli, Frederik Haase, Christian Ochsenfeld and Bettina V. Lotsch. A flavin-inspired covalent organic framework for photocatalytic alcohol oxidation. Chem. Sci., 2021,12, 15143-15150. |
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