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Part 1: Document Description
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Citation |
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Title: |
Replication data for: "Influence of the Template Removal Method on the Mechanical Stability of SBA-15" |
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Identification Number: |
doi:10.18419/darus-2268 |
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Distributor: |
DaRUS |
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Date of Distribution: |
2022-01-28 |
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Version: |
1 |
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Bibliographic Citation: |
Beurer, Ann-Katrin, 2022, "Replication data for: "Influence of the Template Removal Method on the Mechanical Stability of SBA-15"", https://doi.org/10.18419/darus-2268, DaRUS, V1 |
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Citation |
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Title: |
Replication data for: "Influence of the Template Removal Method on the Mechanical Stability of SBA-15" |
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Identification Number: |
doi:10.18419/darus-2268 |
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Authoring Entity: |
Beurer, Ann-Katrin (Institute of Technical Chemistry, University of Stuttgart) |
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Grant Number: |
358283783 - SFB 1333 |
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Distributor: |
DaRUS |
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Access Authority: |
Traa, Yvonne |
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Access Authority: |
Bruckner, Johanna R. |
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Depositor: |
Beurer, Ann-Katrin |
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Date of Deposit: |
2021-12-06 |
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Holdings Information: |
https://doi.org/10.18419/darus-2268 |
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Study Scope |
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Keywords: |
Chemistry, Mechanical Stability, Ordered Mesoporous Silica, Calcination, Soxhlet Extraction |
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Abstract: |
The manuscript describes the influence of the template removal method on the mechanical stability of SBA-15. First, the mechanical stability of calcined SBA-15 was investigated similar to known procedures from literature. The results of the literature were reproduced and confirmed. The main part of the manuscript deals with the mechanical stability of SBA-15, whose pores were opened in different ways - calcination, Soxhlet extraction with ethanol, and Soxhlet extraction with ethanol combined with a thermal treatment in nitrogen.<br> The data used for the manuscript are sorted by the respective characterization method. The data are named according to the sample name (for nomenclature see Notes). The data of the SAXS measurement are sorted by the measurement date. All data are raw data that can be processed with the corresponding software. |
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Kind of Data: |
experimental data |
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Notes: |
<u>Sample nomenclature:</u> <br/> SBA-15-as: directly after the synthesis; called as-synthesized SBA-15<br/> SBA-15-calc: pores were opened by calcination in air<br/> SBA-15-calc-XMPa: pores were opened by calcination, and the sample was pressed with 8 to 156 MPa; abbreviated with “XMPa” depending on the pressure X<br/> SBA-15-calc-re: pores were refilled with Pluronic® P123<br/> SBA-15-calc-re-E: pores were reopened with Soxhlet extraction with ethanol<br/> SBA-15-as-E: pores were opened with Soxhlet extraction with ethanol<br/> SBA-15-as-E-p400: SBA-15-as-E pretreated in N2 at 400°C<br/> SBA-15-as-E-p550: SBA-15-as-E pretreated in N2 at 550°C<br/> File names from SAXS data: The small-anlge X-ray scattering device SAXSess mc2 uses a slit-colimated X-ray beam. Due to this, scattering at the sample leads to a smeared scattering profile with asymmetric scattering maxima. This "smearing" can be removed mathematically by deconvolution of the meassured scattering profile and the intensity profile of the slit-colimated X-ray beam. Thus treated datasets are indicated by the fileextension "deconvoluted". |
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Methodology and Processing |
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Sources Statement |
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Data Access |
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Other Study Description Materials |
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Related Publications |
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Citation |
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Title: |
A.-K. Beurer, J. R. Bruckner, Y. Traa. Influence of the Template Removal Method on the Mechanical Stability of SBA-15. Chemestry Open 2021 10, 1123-1128 |
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Identification Number: |
10.1002/open.202100225 |
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Bibliographic Citation: |
A.-K. Beurer, J. R. Bruckner, Y. Traa. Influence of the Template Removal Method on the Mechanical Stability of SBA-15. Chemestry Open 2021 10, 1123-1128 |
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Label: |
CHN - Elemental analysis.txt |
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Notes: |
text/plain |
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Label: |
SBA-15-as-E-156MPa.RAW |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p400-156MPa.RAW |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p400.RAW |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p550-156MPa.RAW |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p550-39MPa.RAW |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p550.RAW |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E.RAW |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-156MPa.RAW |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-16MPa.RAW |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-39MPa.RAW |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-78MPa.RAW |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-8MPa.RAW |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-re-E-156MPa.RAW |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-re-E.RAW |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc.RAW |
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Notes: |
application/octet-stream |
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Label: |
Cholesteryl palmitate.pdh |
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Notes: |
application/octet-stream |
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Label: |
Cholesteryl palmitate_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
Cholesteryl palmitate.pdh |
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Notes: |
application/octet-stream |
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Label: |
Cholesteryl palmitate_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-156MPa.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-156MPa_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-39MPa.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-39MPa_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-78MPa.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-78MPa_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-8MPa.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-8MPa_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
Cholesteryl palimtate_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
Cholesteryl palmitate.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc_2.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc_2_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc_3.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc_3_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
Cholesteryl palmitate.pdh |
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Notes: |
application/octet-stream |
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Label: |
Cholesteryl palmitate_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-156MPa.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-156MPa_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p400-156MPa.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p400-156MPa_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-re-E-156MPa.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-re-E-156MPa_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
Cholesteryl palmitate.pdh |
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Notes: |
application/octet-stream |
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Label: |
Cholesteryl palmitate_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p400.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p400_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-re-E.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-calc-re-E_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
Cholesteryl palmitate.pdh |
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Notes: |
application/octet-stream |
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Label: |
Cholesteryl palmitate_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p550.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p550_156MPa.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p550_156MPa_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p550_39MPa.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p550_39MPa_deconvoluted.pdh |
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Notes: |
application/octet-stream |
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Label: |
SBA-15-as-E-p550_deconvoluted.pdh |
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Notes: |
application/octet-stream |