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Part 1: Document Description
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Citation |
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Title: |
Replication data of Lotsch group for: "Direct and Linker-Exchange Alcohol-Assisted Hydrothermal Synthesis of Imide-Linked Covalent Organic Frameworks" |
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Identification Number: |
doi:10.18419/darus-2777 |
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Distributor: |
DaRUS |
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Date of Distribution: |
2023-08-02 |
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Version: |
1 |
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Bibliographic Citation: |
Maschita, Johannes; Banerjee, Tanmnay; Lotsch, Bettina V., 2023, "Replication data of Lotsch group for: "Direct and Linker-Exchange Alcohol-Assisted Hydrothermal Synthesis of Imide-Linked Covalent Organic Frameworks"", https://doi.org/10.18419/darus-2777, DaRUS, V1, UNF:6:JpoGE3mNSdR4fNCRgNQIxQ== [fileUNF] |
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Citation |
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Title: |
Replication data of Lotsch group for: "Direct and Linker-Exchange Alcohol-Assisted Hydrothermal Synthesis of Imide-Linked Covalent Organic Frameworks" |
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Identification Number: |
doi:10.18419/darus-2777 |
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Authoring Entity: |
Maschita, Johannes (Max Planck Institute for Solid State Research) |
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Banerjee, Tanmnay (Max Planck Institute for Solid State Research) |
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Lotsch, Bettina V. (Max Planck Institute for Solid State Research) |
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Grant Number: |
358283783 - SFB 1333 |
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Grant Number: |
390776260 - EXC 2089 |
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Grant Number: |
info:eu-repo/grantAgreement/EC/H2020/639233 |
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Grant Number: |
RJF/ 2020/000120 |
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Distributor: |
DaRUS |
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Access Authority: |
Lotsch, Bettina V. |
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Depositor: |
Maschita, Johannes |
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Date of Deposit: |
2022-03-23 |
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Holdings Information: |
https://doi.org/10.18419/darus-2777 |
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Study Scope |
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Keywords: |
Chemistry, Covalent Organic Framework, Hydrothermal Synthesis, Polyimide |
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Abstract: |
Covalent organic frameworks (COFs) are an extensively studied class of porous materials, which distinguish themselves from other porous polymers in their crystallinity and high degree of modularity, enabling a wide range of applications. However, the established synthetic protocols for the synthesis of stable and crystalline COFs, such as imide-linked COFs, often requires the use of high boiling solvents and toxic catalysts, making their synthesis expensive and environmentally harmful. Herein, we report a new environmentally friendly strategy - an alcohol-assisted hydrothermal polymerization approach (aaHTP) for the synthesis of a wide range of crystalline and porous imide-linked COFs. This method allows us to gain access to new COFs and to avoid toxic solvents by up to 90% through substituting commonly used organic solvent mixtures with water and small amounts of n-alcohols without being restricted to water-soluble linker molecules. Additionally, we use the aaHTP to demonstrate an eco-friendly COF-to-COF transformation of an imine-linked COF into a novel imide-linked COF via linkage replacement, inaccessible using published reaction conditions. This dataset contains all data from analytical measurements including FT-IR spectra (*.csv), raw XRRD patterns (*.xyd), 1H, 13C, 15N NMR spectra (*.csv), Ar sorption isotherms (*.txt), TEM images (*.tif), and simulated COF structure files (*.cif) mentioned under the related publication. The data from each anaytical measurement is summarized in a folder named with the measurement. |
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Kind of Data: |
experimental data |
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Kind of Data: |
simulation data |
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Notes: |
View Data by "tree" to understand the file structure and file names according to the designations used in the original publication. |
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Methodology and Processing |
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Sources Statement |
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Data Access |
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Other Study Description Materials |
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Related Publications |
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Citation |
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Title: |
J. Maschita, T. Banerjee, B. V. Lotsch. Direct and Linker-Exchange Alcohol-Assisted Hydrothermal Synthesis of Imide-Linked Covalent Organic Frameworks. Chem. Mater. 2022, 34, 5, 2249-2258. |
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Identification Number: |
10.1021/acs.chemmater.1c04051 |
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Bibliographic Citation: |
J. Maschita, T. Banerjee, B. V. Lotsch. Direct and Linker-Exchange Alcohol-Assisted Hydrothermal Synthesis of Imide-Linked Covalent Organic Frameworks. Chem. Mater. 2022, 34, 5, 2249-2258. |
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File Description--f103273 |
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File: Py-Imide-COF_IR.tab |
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Notes: |
UNF:6:uSuBV8L0p9zb6fp736nzYw== |
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File Description--f103187 |
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File: Py1P-COF_IR.tab |
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Notes: |
UNF:6:xRtt05zls45spVYGZ6S8nw== |
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File Description--f103102 |
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File: TAPA-PMDA-COF_IR.tab |
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Notes: |
UNF:6:AzRiTtjFmwJS1v4SXW1iSw== |
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File Description--f103237 |
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File: TAPB-PMDA-COF_IR.tab |
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Notes: |
UNF:6:KAF4mjICGNr+82498CQ97g== |
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File Description--f103121 |
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File: TAPE-PMDA-COF_IR.tab |
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Notes: |
UNF:6:cy6obdoE4+hDg/n/IQM7FQ== |
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File Description--f103201 |
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File: TAPA-PMDA-COF_water-butanol_precipitate_IR.tab |
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Notes: |
UNF:6:qDdZzSI6ohv8KFHqt0O6aQ== |
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File Description--f103235 |
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File: TAPA-PMDA-COF_water-butanol_supernatant_IR.tab |
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Notes: |
UNF:6:5on1f0HozgdKONHJ/1QWhQ== |
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File Description--f103155 |
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File: TAPA-PMDA-COF_water-ethanol_IR.tab |
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Notes: |
UNF:6:j7oWToNdoS8Pvn4T2fQl5A== |
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File Description--f103119 |
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File: TAPA-PMDA-COF_water-propanol_IR.tab |
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Notes: |
UNF:6:tICaOI58IKS1Oz22X1kdag== |
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File Description--f103104 |
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File: TAPA-PMDA-COF_water_IR.tab |
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Notes: |
UNF:6:tbtPzalIQZ0UG2sSgx+2QQ== |
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File Description--f103254 |
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File: TAPA-PMDA-COF_water_precipitate_IR.tab |
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Notes: |
UNF:6:Gts27nh59WmDgiqsGYyksQ== |
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File Description--f103118 |
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File: TAPA-PMDA-COF_water_supernatant_IR.tab |
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Notes: |
UNF:6:kBLTPJybFJcTgpF/WFkBGA== |
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File Description--f103200 |
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File: TAPA-PMDA_intermediate-salt_IR.tab |
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Notes: |
UNF:6:Y05s6J5i9KQBrCscB5vZ4Q== |
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File Description--f103113 |
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File: TAPB-PMDA-COF_water_IR.tab |
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Notes: |
UNF:6:J121A14P3Nnhl+HUi5UnrA== |
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File Description--f103252 |
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File: PMDA_IR.tab |
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Notes: |
UNF:6:53wh4ht+mOZ6ZKx5gdlsmg== |
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File Description--f103211 |
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File: TAPA_IR.tab |
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Notes: |
UNF:6:cykbTCiT0kgUm782yc9vFw== |
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File Description--f103218 |
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File: TAPB_IR.tab |
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Notes: |
UNF:6:GK/vIsZwQh1P3Wyeg8rWQQ== |
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File Description--f103275 |
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File: TAPE_IR.tab |
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Notes: |
UNF:6:YXHVQul4mZ3+dbSXuM0p8g== |
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File Description--f103270 |
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File: Py-Imide-COF_classical_solvothermal.tab |
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Notes: |
UNF:6:NotlcManeA1O+gHnDSGuRw== |
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File Description--f103163 |
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File: Py-Imide-COF_direct_aaHTP.tab |
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Notes: |
UNF:6:hreRZIWazJxFW7VtZIPKPQ== |
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File Description--f103264 |
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File: Py-Imide-COF_ionothermal_eutectic_salt_mixture.tab |
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Notes: |
UNF:6:3Zji9mMOVqpBZ/ZudHCKXA== |
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File Description--f103103 |
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File: Py-Imide-COF_ionothermal_ZnCl2.tab |
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Notes: |
UNF:6:69Xyui/+O2adhQS78SMNLg== |
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File Description--f103267 |
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File: TAPE-PMDA-COF_classical_solvothermal.tab |
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Notes: |
UNF:6:r/luKrPjX3VmNr8SdqZUvw== |
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File Description--f103127 |
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File: TAPE-PMDA-COF_hydrothermal.tab |
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Notes: |
UNF:6:cy6obdoE4+hDg/n/IQM7FQ== |
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File Description--f103246 |
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File: TAPE-PMDA-COF_ionothermal_eutectic_salt_mixture.tab |
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Notes: |
UNF:6:g6MEOEByRsitB+4b8/GBfA== |
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File Description--f103161 |
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File: TAPE-PMDA-COF_ionothermal_ZnCl2.tab |
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Notes: |
UNF:6:aGn5mqwcxJa02BJ8Z1qicA== |
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File Description--f103216 |
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File: Py-Imide-COF_13C_ssNMR.tab |
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Notes: |
UNF:6:4U7CI6rnEvexpqjLeV8ovw== |
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File Description--f103202 |
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File: Py1P-COF_13C_ssNMR.tab |
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Notes: |
UNF:6:mZFmOqFstLZpIh9sNTTFpQ== |
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File Description--f103179 |
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File: TAPA-PMDA-COF_13C_ssNMR.tab |
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Notes: |
UNF:6:lqRo/gqb3NRuEvLUS6PlNw== |
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File Description--f103146 |
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File: TAPB-PMDA-COF_13C_ssNMR.tab |
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Notes: |
UNF:6:B2LgJ0LOZJ8Zht792gAT8w== |
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File Description--f103257 |
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File: TAPE-PMDA-COF_13C_ssNMR.tab |
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Notes: |
UNF:6:Aj92AtG4C/M4ilXqBQLLBA== |
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File Description--f103208 |
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File: Py-Imide-COF_15N_ssNMR.tab |
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Notes: |
UNF:6:wo/MOfu2mIMQuGgeXXAyfw== |
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File Description--f103240 |
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File: Py1P-COF_15N_ssNMR.tab |
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Notes: |
UNF:6:njE6AtPURtqtNVDLbPr2tg== |
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File Description--f103177 |
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File: Species_in_supernatant_1H_NMR.tab |
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Notes: |
UNF:6:pYDY1c44RUgyxVHGk9jF4g== |
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Label: |
Py-Imide-COF.cif |
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Notes: |
chemical/x-cif |
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Label: |
Py1P-COF.cif |
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Notes: |
chemical/x-cif |
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Label: |
TAPA-PMDA-COF.cif |
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Notes: |
chemical/x-cif |
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Label: |
TAPB-PMDA-COF.cif |
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Notes: |
chemical/x-cif |
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Label: |
TAPE-PMDA-COF.cif |
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Notes: |
chemical/x-cif |
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Py-Imide-COF_BET_Ar.txt |
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text/plain |
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Py-Imide-COF_Isotherme_Ar.txt |
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text/plain |
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Py-Imide-COF_PSD_Ar.txt |
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text/plain |
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Py1P-COF_BET_Ar.txt |
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text/plain |
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Py1P-COF_Isotherme_Ar.txt |
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text/plain |
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Py1P-COF_PSD_Ar.txt |
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text/plain |
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TAPA-PMDA-COF_BET_Ar.txt |
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text/plain |
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TAPA-PMDA-COF_Isotherme_Ar.txt |
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text/plain |
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TAPA-PMDA-COF_PSD_Ar.txt |
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TAPB-PMDA-COF_BET_Ar.txt |
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TAPB-PMDA-COF_Isotherme_Ar.txt |
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TAPB-PMDA-COF_PSD_Ar.txt |
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TAPE-PMDA-COF_BET_Ar.txt |
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TAPE-PMDA-COF_Isotherm_Ar.txt |
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TAPE-PMDA-COF_PSD_Ar.txt |
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TAPA-PMDA-COF_10percent_HexOH_BET_Ar.txt |
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TAPA-PMDA-COF_10percent_HexOH_Isotherme_Ar.txt |
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TAPA-PMDA-COF_10percent_HexOH_PSD_Ar.txt |
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TAPA-PMDA-COF_20percent_ButOH_BET_Ar.txt |
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TAPA-PMDA-COF_20percent_ButOH_Isotherme_Ar.txt |
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TAPA-PMDA-COF_20percent_ButOH_PSD_Ar.txt |
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TAPA-PMDA-COF_20percent_HexOH_BET_Ar.txt |
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TAPA-PMDA-COF_20percent_HexOH_Isotherme_Ar.txt |
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TAPA-PMDA-COF_20percent_HexOH_PSD_Ar.txt |
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TAPA-PMDA-COF_20percent_PentOH_BET_Ar.txt |
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TAPA-PMDA-COF_20percent_PentOH_Isotherme_Ar.txt |
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TAPA-PMDA-COF_20percent_PentOH_PSD_Ar.txt |
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TAPA-PMDA-COF_30percent_ButOH_BET_Ar.txt |
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TAPA-PMDA-COF_30percent_ButOH_Isotherme_Ar.txt |
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TAPA-PMDA-COF_30percent_ButOH_PSD_Ar.txt |
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TAPA-PMDA-COF_30percent_PrOH_BET_Ar.txt |
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TAPA-PMDA-COF_30percent_PrOH_Isotherme_Ar.txt |
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TAPA-PMDA-COF_30percent_PrOH_PSD_Ar.txt |
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TAPA-PMDA-COF_0mul pyridine_BET_Ar.txt |
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TAPA-PMDA-COF_0mul pyridine_Isotherme_Ar.txt |
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TAPA-PMDA-COF_0mul pyridine_PSD_Ar.txt |
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TAPA-PMDA-COF_10mul pyridine_BET_Ar.txt |
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TAPA-PMDA-COF_10mul pyridine_Isotherme_Ar.txt |
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TAPA-PMDA-COF_10mul pyridine_PSD_Ar.txt |
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TAPA-PMDA-COF_20mul pyridine_BET_Ar.txt |
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TAPA-PMDA-COF_20mul pyridine_Isotherme_Ar.txt |
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TAPA-PMDA-COF_20mul pyridine_PSD_Ar.txt |
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TAPA-PMDA-COF_40mul pyridine_BET_Ar.txt |
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TAPA-PMDA-COF_40mul pyridine_Isotherme_Ar.txt |
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TAPA-PMDA-COF_40mul pyridine_PSD_Ar.txt |
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TAPA-PMDA-COF_24 hours_BET_Ar.txt |
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TAPA-PMDA-COF_24 hours_Isotherme_Ar.txt |
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TAPA-PMDA-COF_24 hours_PSD_Ar.txt |
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Py-Imide-COF_TEM_1.tif |
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Py-Imide-COF_TEM_2.tif |
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Py1P-COF_TEM_1.tif |
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TAPA-PMDA-COF_TEM_1.tif |
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TAPA-PMDA-COF_TEM_2.tif |
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TAPB-PMDA-COF_TEM_1.tif |
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TAPB-PMDA-COF_TEM_2.tif |
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TAPE-PMDA-COF_TEM_1.tif |
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Py-Imide-COF_XRPD.xyd |
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Py1P-COF_XRPD.xyd |
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TAPA-PMDA-COF_100percent_ButOH_XRPD.xyd |
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TAPA-PMDA-COF_100percent_HexOH_XRPD.xyd |
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Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_100percent_PrOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_100percent_water_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_10percent_ButOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_10percent_HexOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_10percent_PentOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_10percent_PrOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_20percent_ButOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_20percent_HexOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_20percent_PentOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_20percent_PrOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_30percent_ButOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_30percent_PrOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_50percent_EtOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_50percent_PrOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_5percent_ButOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_5percent_HexOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_70percent_PrOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_0mul pyridine_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_10mul pyridine_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_20mul pyridine_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_40mul pyridine_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_120C_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_140C_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_160C_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_180C_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_15 hours_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_24 hours_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_4 days_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPB-PMDA-COF_100percent_water_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_crystalline_from_amorphous_PI_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_water-butanol_precipitate_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_water_precipitate_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA_intermediate-salt_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
Py-Imide-COF_classical_solvothermal_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
Py-Imide-COF_direct_aaHTP_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
Py-Imide-COF_ionothermal_eutectic_salt_mixture_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
Py-Imide-COF_ionothermal_ZnCl2_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
Py-Imide-COF_12M_HCl.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
Py-Imide-COF_50%_HCOOH.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
Py-Imide-COF_pristine.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
Py1P-COF_12M_HCl.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
Py1P-COF_50%_HCOOH.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
Py1P-COF_pristine.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_20%_HexOH_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPA-PMDA-COF_recycled_organic_phase_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPE-PMDA-COF_classical_solvothermal_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPE-PMDA-COF_hydrothermal_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPE-PMDA-COF_ionothermal_eutectic_salt_mixture_XRPD.xyd |
|
Notes: |
application/octet-stream |
|
Label: |
TAPE-PMDA-COF_ionothermal_ZnCl2_XRPD.xyd |
|
Notes: |
application/octet-stream |