Publication data for: "From Macro to Mesoporous ZnO Inverse Opals: Synthesis, Characterization and Tracer Diffusion Properties"doi:10.18419/darus-1399DaRUS2021-04-151Kousik, Shravan R., 2021, "Publication data for: "From Macro to Mesoporous ZnO Inverse Opals: Synthesis, Characterization and Tracer Diffusion Properties"", https://doi.org/10.18419/darus-1399, DaRUS, V1, UNF:6:hD14tiP+DJV00NtMt0Oifw== [fileUNF]Publication data for: "From Macro to Mesoporous ZnO Inverse Opals: Synthesis, Characterization and Tracer Diffusion Properties"doi:10.18419/darus-1399Kousik, Shravan R.358283783 - SFB 1333DaRUSAtanasova, PetiaKousik, Shravan R.2021-02-18ChemistryZnO Inverse OpalsMesoporous materialsDiffusion in poresFluorescence correlation spectroscopyThis paper describes the synthesis and characterization of macro-mesoporous ZnO inverse opals through a template-based approach. In addition, the distribution and diffusion of a fluorescent organic tracer molecule (Alexa Fluor 488) through quasi-mesoporous ZnO inverse opals was investigated via confocal laser scanning microscopy (CLSM) and fluorescence correlation spectroscopy (FCS). The attached data consists of relevant scanning electron microscope (SEM) images, particle and pore-size distributions, film thickness data, X-ray diffraction (XRD) patterns, ultraviolet-visible (UV-Vis) spectra, CLSM images and FCS spectra. The following data formats are used: *tif, *.png, *.xlsx and *.xy. The data files are ordered as per their appearance in the publication.Kousik, S.R.; Sipp, D.; Abitaev, K.; Li, Y.; Sottmann, T.; Koynov, K.; Atanasova, P. From Macro to Mesoporous ZnO Inverse Opals: Synthesis, Characterization and Tracer Diffusion Properties. Nanomaterials 2021, 11, 196.10.3390/nano11010196Kousik, S.R.; Sipp, D.; Abitaev, K.; Li, Y.; Sottmann, T.; Koynov, K.; Atanasova, P. From Macro to Mesoporous ZnO Inverse Opals: Synthesis, Characterization and Tracer Diffusion Properties. Nanomaterials 2021, 11, 196.Fig.7b - Alexa 488 above ZnO-IO.tab1404text/tab-separated-valuesUNF:6:lJb8IHkW5SV7jNqn12nIIg==Fig.7b - Alexa 488 in ZnO-IO.tab1844text/tab-separated-valuesUNF:6:ob6K7jQnrr6aW5TR9SKJ1Q==Fig.S5b.tab612text/tab-separated-valuesUNF:6:ibqdnsc9L03zuhyujGZlsw==Fig.6b - UV.tab6013text/tab-separated-valuesUNF:6:/NFn0B05nmZPM9s5Bc7Lzg==Fig.5 - XRD-ZnO-standard-ICSD-34477.tab6102text/tab-separated-valuesUNF:6:ql29qEJxzRubiF1/QtpxFw==Lag Time (s)0.0421429656285854660.20972.1.0E-65.375E-4140.00.00.018724477142857146UNF:6:7sKGK7LMGQNysGXp2uEv1w==Correlation0.0381350.0-0.001291.04875.0.3503621338263489140.00.2604147804285714UNF:6:Kbs1qQrEpk/EU1nDFu3ucA==Lag Time Fit (s)0.0140.05.375E-4.0.0421429656285854660.209720.0187244771428571461.0E-6UNF:6:7sKGK7LMGQNysGXp2uEv1w==Correlation Fit9.79E-60.344489948443250650.9894140.00.039270.2577848527857142.0.0UNF:6:B3tE1EagE2OrDpz2a8HzFg==Lag Time (s)0.00255999999999999986.710890.455902547826087184.00.0.2.0E-71.2029355997817777UNF:6:eu+4kpuv+RspjdoN5oQlSA==Correlation184.01.244270.26085.0.334914987200415240.0-0.003260.34788187499999995UNF:6:Xl4tdK1zIh8g1Fxb3M66Ng==Lag Time Fit (s)UNF:6:+ce67cnscg4zdnAMzP1FWg==Correlation FitUNF:6:rLZbnolC3YGFy8PajN5aPw==Position Z (µm)23.868.876467014903321-6.148.860.08.86000000000000361.0.UNF:6:uC66RkjiJECaYVeZAdvjWg==Count rate (kHz).0.55725498502331361.48561.115661.04.1981.59890.0UNF:6:fd9F5wm5tgFD64erQ2rD5g==Wavelength (nm)0.0.500.0800.0200.0601.0173.63803346809323500.0UNF:6:HxcXsODgybUEvSM9ihthIw==% Reflectance (5c ZnO-extraction)3.714810.60310527592119824.4203341430948450.6859427.45749.601.00.0UNF:6:OpuXX6Rur2NsPMbyCiYKDg==% Reflectance (5c ZnO-calcination)6.169102040687992601.04.353422.4576.17.7176481031613950.021.82215UNF:6:WRjv9Q1EwY5NiKxuT8xSfw==2-Theta20.0.50.45610.080.950.4517.6236110563830480.0UNF:6:eYqTM0IUaKBui1aY/pKZnw==Intensity0.09074.0.610.00.0132.119672131147580.0701.547768415919UNF:6:6f/fYpHr73C0+PdEki2UBQ==Fig.7a - Image 19 3D.pngCLSM image of multilayered ZnO inverse opals with a pore size of 60 nm infiltrated with Alexa Fluor 488image/pngFig.7b - Alexa 488 above ZnO-IO.xlsxNormalized autocorrelation function for Alexa Fluor 488 diffusing in waterapplication/vnd.openxmlformats-officedocument.spreadsheetml.sheetFig.7b - Alexa 488 in ZnO-IO.xlsxNormalized autocorrelation function for Alexa Fluor 488 diffusing in ZnO-IOapplication/vnd.openxmlformats-officedocument.spreadsheetml.sheetFig.S5b.xlsxRaw data - Fluorescence intensity scan through ZnO IO film immersed in Alexa Fluor 488 in a direction normal to the film planeapplication/vnd.openxmlformats-officedocument.spreadsheetml.sheetFig.S1a - PS 60 nm.xlsxThickness of 60 nm PS template filmsapplication/vnd.openxmlformats-officedocument.spreadsheetml.sheetFig.S1b - PS 70 nm.xlsxThickness of 70 nm PS template filmsapplication/vnd.openxmlformats-officedocument.spreadsheetml.sheetFig.S1c - PS 175 nm.xlsxThickness of 175 nm PS template filmsapplication/vnd.openxmlformats-officedocument.spreadsheetml.sheetFig.2a-d - PS particle and inverse opal pore size distributions.xlsxAverage diameters, standard deviations and polydispersities of PS particles and the pores of their corresponding ZnO inverse opals application/vnd.openxmlformats-officedocument.spreadsheetml.sheetTable 2 - PS particles and ZnO IO pore size statistics.xlsxAverage diameters, standard deviations and polydispersities of PS particles and the pores of their corresponding ZnO inverse opalsapplication/vnd.openxmlformats-officedocument.spreadsheetml.sheetFig.1b - PS template 175 nm.tifSEM - PS175-T (175 nm PS particles)image/tiffFig.1c - PS template 70 nm.tifSEM - PS70-T (70 nm PS particles)image/tiffFig.1d - PS template 60 nm.tifSEM - PS60-T (60 nm PS particles)image/tiffFig.1e - PS template 48 nm.tifSEM - PS48-T (48 nm PS particles)image/tiffFig.1f - ZnO inverse opal 131 nm.tifSEM - Z175-IO (ZnO inverse opals with pore size : 131 nm)image/tiffFig.1g - ZnO inverse opal 60 nm.tifSEM - Z70-IO (ZnO inverse opals with pore size : 60 nm)image/tiffFig.1h - ZnO inverse opal 50 nm.tifSEM - Z60-IO (ZnO inverse opals with pore size : 50 nm)image/tiffFig.1i - ZnO inverse opal Z48-IO.tifSEM - Z48-IO (ZnO inverse opals)image/tiffFig.3a - ZnO inverse opal with 60 nm PS template.tifSEM - Z60-IO (ZnO inverse opals obtained from 60 nm PS particles) - Infiltration depthimage/tiffFig.3b - ZnO inverse opal with 175 nm PS template.tifCross-section SEM - Z175-IO (ZnO inverse opals obtained from 175 nm PS particles)image/tiffFig.4a - PS template 70 nm.tifCross-section SEM - PS70-Timage/tiffFig.4b - ZnO inverse opal-calcined.tifCross-section SEM - Z70-IO - Calcinedimage/tiffFig.4c - ZnO inverse opal-solvent extraction.tifCross-section SEM - Z70-IO - Extractedimage/tiffFig.4d - ZnO inverse opal-calcinated-additional 1 cycle ZnO.tifCross-section SEM - Z70-IO - Calcined - 1 additional ZnO deposition cycleimage/tiffFig.4e - ZnO inverse opal-solvent extraction-additional 1 cycle ZnO.tifCross-section SEM - Z70-IO - Extracted - 1 additional ZnO deposition cycleimage/tiffFig.4f - ZnO inverse opal-calcined-additional 2 cycles ZnO.tifCross-section SEM - Z70-IO - Calcined - 2 additional ZnO deposition cyclesimage/tiffFig.4g - ZnO inverse opal-solvent extraction-additional 2 cycles ZnO.tifCross-section SEM - Z70-IO - Extracted - 2 additional ZnO deposition cyclesimage/tiffFig.6a - PS template 175 nm.tifSEM image of PS template with diameter 175 nmimage/tiffFig.S2 - 175 nm PS template film - crack formation.tifCross-section SEM - PS175-Timage/tiffFig.S3a - ZnO-IO pore size 131 nm 3 cycles ZnO-calcined.tifCross-section SEM image of Z175-IO after 3 mineralization cycles followed by calcinationimage/tiffFig.S3b - ZnO-IO pore size 131 nm 3 cycles ZnO-solvent extraction.tifCross-section SEM image of Z175-IO after 3 mineralization cycles followed by extractionimage/tiffFig.S4a - ZnO-IO pore size 50 nm-calcined.tifCross-section SEM image of Z60-IO after 3 mineralization cycles followed by calcinationimage/tiffFig.S5a - Multilayered ZnO-IO pore size 60 nm.tifCross-section SEM - Multilayered ZnO IO for CLSMimage/tiffFig.6b - UV.xlsxRaw data for UV-Vis spectra of Z175-IO obtained after extraction and calcinationapplication/vnd.openxmlformats-officedocument.spreadsheetml.sheetFig.6c - UV.xlsxRaw data for UV-Vis spectra of Z175-IO obtained after extraction measured at different angles of incidenceapplication/vnd.openxmlformats-officedocument.spreadsheetml.sheetFig.5 - XRD-ZnO-5c-175nm-Calcined.xyRaw data - XRD - Z175-IO after calcinationapplication/octet-streamFig.5 - XRD-ZnO-5c-175nm-Extracted.xyRaw data - XRD - Z175-IO - After Extractionapplication/octet-streamFig.5 - XRD-ZnO-standard-ICSD-34477.xlsxRaw data - XRD - ZnO - ICSD number : 34477application/vnd.openxmlformats-officedocument.spreadsheetml.sheet