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Part 1: Document Description
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Citation |
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Title: |
Replication Data for: Synthesis of Tungsten(VI) Imido Alkylidene Bispyrrolide Complexes via the Isocyanate Route |
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Identification Number: |
doi:10.18419/darus-1670 |
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Distributor: |
DaRUS |
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Date of Distribution: |
2021-03-19 |
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Version: |
1 |
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Bibliographic Citation: |
Musso, Janis; Benedikter, Mathis; Gebel, Paul; Elser, Iris; Frey, Wolfgang; Buchmeiser, Michael, 2021, "Replication Data for: Synthesis of Tungsten(VI) Imido Alkylidene Bispyrrolide Complexes via the Isocyanate Route", https://doi.org/10.18419/darus-1670, DaRUS, V1 |
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Citation |
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Title: |
Replication Data for: Synthesis of Tungsten(VI) Imido Alkylidene Bispyrrolide Complexes via the Isocyanate Route |
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Identification Number: |
doi:10.18419/darus-1670 |
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Authoring Entity: |
Musso, Janis (Universität Stuttgart) |
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Benedikter, Mathis (Universität Stuttgart) |
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Gebel, Paul (Universität Stuttgart) |
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Elser, Iris (Universität Stuttgart) |
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Frey, Wolfgang (Universität Stuttgart) |
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Buchmeiser, Michael (Universität Stuttgart) |
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Grant Number: |
U2174/22-1 |
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Grant Number: |
58283783-CRC1333 |
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Distributor: |
DaRUS |
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Access Authority: |
Buchmeiser, Michael |
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Depositor: |
Musso, Janis |
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Date of Deposit: |
2021-03-09 |
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Holdings Information: |
https://doi.org/10.18419/darus-1670 |
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Study Scope |
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Keywords: |
Chemistry, Tungsten, Alkylidene Group, Isocyanates |
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Abstract: |
A general route to tungsten(VI) imido alkylidene bispyrrolide complexes via the extrusion of CO2 from the reaction of one equivalent of an aryl isocyanate with WOCl4 to form the corresponding imido complexes is reported. The Dataset contains the NMR spectra of figures S1 and S2 (zip-file 1 and 2) and NMR spectra of all compounds (zip-file 3). The detailed procedure for the synthesis of compunds as well as information about the used analytical equipment can be found in the supporting information of the paper. |
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Methodology and Processing |
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Sources Statement |
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Data Access |
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Other Study Description Materials |
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Related Studies |
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Single Crystal x-ray structure of W(N-2,6-Cl2-C6H3)(CH2Ph)3(OtBu): <a href="https://doi.org/10.5517/ccdc.csd.cc25jn8n">DOI: 10.5517/ccdc.csd.cc25jn8n</a> |
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Single Crystal x-ray structure of compund W-13: <a href="https://doi.org/10.5517/ccdc.csd.cc25jnbq">DOI: 10.5517/ccdc.csd.cc25jnbq</a> |
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Single Crystal x-ray structure of compund W-4a: <a href="https://doi.org/10.5517/ccdc.csd.cc25jncr">DOI: 10.5517/ccdc.csd.cc25jncr</a> |
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Related Publications |
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Citation |
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Title: |
Janis V. Musso, Mathis J. Benedikter, Paul Gebel, Iris Elser, Wolfgang Frey, and Michael R. Buchmeiser. Synthesis of Tungsten(VI) Imido Alkylidene Bispyrrolide Complexes via the Isocyanate Route. Organometallics 2020 39 (17), 3072-3076 |
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Identification Number: |
10.1021/acs.organomet.0c00435 |
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Bibliographic Citation: |
Janis V. Musso, Mathis J. Benedikter, Paul Gebel, Iris Elser, Wolfgang Frey, and Michael R. Buchmeiser. Synthesis of Tungsten(VI) Imido Alkylidene Bispyrrolide Complexes via the Isocyanate Route. Organometallics 2020 39 (17), 3072-3076 |
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Label: |
Figure S1.zip |
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Notes: |
application/zip |
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Label: |
Figure S2.zip |
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Notes: |
application/zip |
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Label: |
spectra of compounds.zip |
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Notes: |
application/zip |