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Part 1: Document Description
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Citation |
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Title: |
Replication data of B3 group for: "Interplay of Polarity and Confinement in Asymmetric Catalysis with Chiral Rh Diene Complexes in Microemulsions" |
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Identification Number: |
doi:10.18419/darus-2210 |
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Distributor: |
DaRUS |
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Date of Distribution: |
2022-02-21 |
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Version: |
1 |
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Bibliographic Citation: |
Kirchhof, Manuel, 2022, "Replication data of B3 group for: "Interplay of Polarity and Confinement in Asymmetric Catalysis with Chiral Rh Diene Complexes in Microemulsions"", https://doi.org/10.18419/darus-2210, DaRUS, V1 |
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Citation |
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Title: |
Replication data of B3 group for: "Interplay of Polarity and Confinement in Asymmetric Catalysis with Chiral Rh Diene Complexes in Microemulsions" |
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Identification Number: |
doi:10.18419/darus-2210 |
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Authoring Entity: |
Kirchhof, Manuel (University of Stuttgart, Institute of Organic Chemistry) |
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Grant Number: |
358283783 - SFB 1333 |
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Distributor: |
DaRUS |
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Access Authority: |
Laschat, Sabine |
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Depositor: |
Kirchhof, Manuel |
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Date of Deposit: |
2021-10-21 |
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Holdings Information: |
https://doi.org/10.18419/darus-2210 |
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Study Scope |
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Keywords: |
Chemistry, Asymmetric Catalysis, Rhodium Catalysis, Anion Exchange, Amphiphilic Film, C-C Coupling, Diene Ligands, Kinetics, Liquid Confinement, Microemulsion |
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Abstract: |
In this dataset HPLC (high performance liquid chromatography) chromatograms of the products of the rhodium-catalyzed 1,2-addition and NMR spectra of all prepared ligands, catalysts and catalysis products (NMR) are included. Furthermore, the NMR data of temperature and solvent dependent kinetics in dioxane and in microemulsions (Kinetiken) are listed. Crystallographic data was published in Cambridge Structural Database (CSD) of the Cambridge Crystallographic Data Centre (CCDC) as stated under related datasets. |
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Kind of Data: |
experimental data |
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Kind of Data: |
analytical data |
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Methodology and Processing |
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Sources Statement |
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Data Access |
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Other Study Description Materials |
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Related Studies |
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Structure L2-H2: CCDC 2099410 doi: <a href="https://doi.org/10.5517/ccdc.csd.cc28glx8">10.5517/ccdc.csd.cc28glx8</a> |
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<br/>Structure L1-H2: CCDC 2099412 doi: <a href="https://doi.org/10.5517/ccdc.csd.cc28glzb">10.5517/ccdc.csd.cc28glzb</a> |
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<br/>Structure [Rh(L2)OTf]: CCDC 2099413 doi: <a href="https://doi.org/10.5517/ccdc.csd.cc28gm0d">10.5517/ccdc.csd.cc28gm0d</a> |
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<br/>Structure [Rh(L2)OTs]: CCDC 2099414, <a href="https://doi.org/10.5517/ccdc.csd.cc28gm1f">10.5517/ccdc.csd.cc28gm1f</a> |
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<br/>Structure [Rh(L2)OAc]: CCDC 2099419, doi: <a href="https://doi.org/10.5517/ccdc.csd.cc28gm6l">10.5517/ccdc.csd.cc28gm6l</a> |
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<br/>Structure [Rh(L2)PO2F2]: CCDC 2099420 doi: <a href="https://doi.org/10.5517/ccdc.csd.cc28gm7m">10.5517/ccdc.csd.cc28gm7m</a> |
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<br/>Structure [[Rh(L2)OH2]SbF6 · CH2Cl2]: CCDC 2099421 doi: <a href="https://doi.org/10.5517/ccdc.csd.cc28gm8n">10.5517/ccdc.csd.cc28gm8n</a> |
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Related Publications |
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Citation |
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Title: |
Manuel Kirchhof, Karina Abitaev, Abdulwahab Abouhaileh, Katrin Gugeler, Wolfgang Frey, Anna Zens, Johannes Kästner, Thomas Sottmann, Sabine Laschat. Interplay of Polarity and Confinement in Asymmetric Catalysis with Chiral Rh Diene Complexes in Microemulsions. Chem. Eur. J. 2021, 68, 16853-16870. |
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Identification Number: |
10.1002/chem.202102752 |
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Bibliographic Citation: |
Manuel Kirchhof, Karina Abitaev, Abdulwahab Abouhaileh, Katrin Gugeler, Wolfgang Frey, Anna Zens, Johannes Kästner, Thomas Sottmann, Sabine Laschat. Interplay of Polarity and Confinement in Asymmetric Catalysis with Chiral Rh Diene Complexes in Microemulsions. Chem. Eur. J. 2021, 68, 16853-16870. |
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[Rh(COD)Cl] in C8G1 ME (28).xps |
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[Rh(L1)Cl] in C8G1,AOT ME (14,5).xps |
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[Rh(L1)Cl] in C8G1,AOT ME (21,5).xps |
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[Rh(L2)Cl]2 in C8G1,SDS ME (28,5).xps |
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[Rh(L2)OAc] in C8G1 ME (28).xps |
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[Rh(L2)OAc] in C8G1,AOT ME (14,5).xps |
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[Rh(L2)OAc] in C8G1,AOT ME (21,5).xps |
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[Rh(L2)OAc] in C8G1,DTAB ME (28,10).xps |
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[Rh(L2)OAc] in C8G1,SDS ME (14,10).xps |
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[Rh(L2)OAc] in C8G1,SDS ME (28,10).xps |
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[Rh(L2)OAc] in C8G1,SDS ME (28,5).xps |
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[Rh(L2)OAc] in Toluol,H2O, 1 Äq AOT.xps |
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[Rh(L2)OAc] in Toluol,H2O, 1 Äq SDS.xps |
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[Rh(L2)OAc] in Toluol,H2O, 30 mg AOT.xps |
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[Rh(L2)OAc] in Toluol,H2O, 30 mg SDS.xps |
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[Rh(L2)OAc] with 2 x cmc C8G1.xps |
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[Rh(L2)OH2]SbF6 in C8G1 ME (28).xps |
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[Rh(L2)OH2]SbF6 in C8G1,AOT ME (14,5).xps |
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[Rh(L2)OH2]SbF6 in C8G1,AOT ME (21,5).xps |
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[Rh(L2)OH2]SbF6 in C8G1,AOT ME (28,5).xps |
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[Rh(L2)OH2]SbF6 in dioxane.xps |
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[Rh(L2)OTf] in C8G1 ME (28).xps |
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[Rh(L2)OTf] in C8G1,AOT ME (14,5).xps |
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[Rh(L2)OTf] in C8G1,AOT ME (21,5).xps |
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[Rh(L2)OTf] in C8G1,AOT ME (28,5).xps |
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[Rh(L2)OTf] in dioxane.xps |
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[Rh(L2)OTs] in C8G1 ME (28).xps |
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[Rh(L2)OTs] in C8G1,AOT ME (14,5).xps |
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[Rh(L2)OTs] in C8G1,AOT ME (21,5).xps |
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[Rh(L2)OTs] in C8G1,AOT ME (28,5).xps |
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[Rh(L2)OTs] in C8G1,SDS ME (14,10).xps |
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[Rh(L2)OTs] in C8G1,SDS ME (28,10).xps |
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[Rh(L2)OTs] in C8G1,SDS ME (28,5).xps |
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[Rh(L2)OTs] in dioxan.xps |
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[Rh(L2)PO2F2] in C8G1 ME (28).xps |
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[Rh(L2)PO2F2] in dioxane.xps |
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2 x CMC at 50 °C with [Rh(L2)OAc].zip |
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dioxane at 60 °C with [Rh(L2)OAc].zip |
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gamma = 14 delta = 5 at 50 °C with [Rh(L2)OAc].zip |
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gamma = 21 delta = 5 at 50 °C with [Rh(L2)OAc].zip |
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gamma = 28 at 40 °C with [Rh(L2)OAc].zip |
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gamma = 28 at 50 °C with [Rh(L2)OAc].zip |
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gamma = 28 at 60 °C with [Rh(L2)OAc].zip |
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gamma = 28 delta = 5 at 50 °C with [Rh(L2)OAc].zip |
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3.zip |
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L1-H2.zip |
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L2-H2.zip |
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[Rh(L2)AOT].zip |
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application/zip |
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[Rh(L2)OAc].zip |
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application/zip |
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[Rh(L2)OH2]SbF6.zip |
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[Rh(L2)OTf].zip |
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[Rh(L2)OTs].zip |
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[Rh(L2)PO2F2].zip |
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application/zip |
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[Rh(L2)SDS].zip |
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application/zip |
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Counterion Exchange-1.zip |
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Hydrogenation Products.zip |
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application/zip |