Data from Bill group for: Hierarchical Silica Inverse Opals as a Catalyst Support for Asymmetric Molecular Heterogeneous Catalysis with Chiral Rh-diene Complexes (doi:10.18419/darus-1788)

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Data from Bill group for: Hierarchical Silica Inverse Opals as a Catalyst Support for Asymmetric Molecular Heterogeneous Catalysis with Chiral Rh-diene Complexes

doi:10.18419/darus-1788

DaRUS

2021-04-14

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Atanasova, Petia, 2021, "Data from Bill group for: Hierarchical Silica Inverse Opals as a Catalyst Support for Asymmetric Molecular Heterogeneous Catalysis with Chiral Rh-diene Complexes", https://doi.org/10.18419/darus-1788, DaRUS, V1

Data from Bill group for: Hierarchical Silica Inverse Opals as a Catalyst Support for Asymmetric Molecular Heterogeneous Catalysis with Chiral Rh-diene Complexes

doi:10.18419/darus-1788

Atanasova, Petia (University of Stuttgart)

358283783 - SFB 1333

DaRUS

Bill, Joachim

Atanasova, Petia

2021-04-12

https://doi.org/10.18419/darus-1788

Chemistry, Silica inverse opals, Confocal Laser Scanning Microscopy (CLSM)

Inorganic chemistry

This dataset contains primary and processed data files obtained by the Bill group for the related publication. The data from the other collaborating groups are included in a separate dataset. This dataset consists of scanning electron microscopy (SEM), confocal laser scanning microscopy (SEM) and Brunauer-Emmett-Teller (BET) nitrogen sorption data. The following data formats are used: *.tif, *.png, *.pdf, and *.lsm. The dataset follows the same labelling as the publication.

Experimental data

CLSM images saved as *.lsm files can be opened with the original software of the microscope ZEN (Carl Zeiss, Jena, Germany) or with the open access program ImageJ (<a href="https://imagej.nih.gov/ij/download.html">https://imagej.nih.gov/ij/download.html</a>).

Max Deimling, Shravan R. Kousik, Karina Abitaev, Wolfgang Frey, Thomas Sottmann, Kaloian Koynov, Sabine Laschat and Petia Atanasova. Hierarchical Silica Inverse Opals as a Catalyst Support for Asymmetric Molecular Heterogeneous Catalysis with Chiral Rh-diene Complexes. ChemCatChem, 2021, 13 , 1-12.

10.1002/cctc.202001997

Max Deimling, Shravan R. Kousik, Karina Abitaev, Wolfgang Frey, Thomas Sottmann, Kaloian Koynov, Sabine Laschat and Petia Atanasova. Hierarchical Silica Inverse Opals as a Catalyst Support for Asymmetric Molecular Heterogeneous Catalysis with Chiral Rh-diene Complexes. ChemCatChem, 2021, 13 , 1-12.

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Figure 5 - BET and BJH.pdf

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BET analysis of bulk macro-mesoporous silica inverse opal

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Figure S2 - BET.pdf

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BET analysis of silica support Si-IO-L1 after the 5th catalytic reaction

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Figure 2a - CLSM image of silica inverse opal - lower magnification.tif

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CLSM image of silica inverse opal infiltrated with PL silane probe molecule 6

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Figure 2a - raw data.lsm

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CLSM image of silica inverse opal infiltrated with PL silane probe molecule 6 - raw data

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Figure 2b - CLSM image of silica inverse opal - higher magnification.tif

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CLSM image od silica inverse opal infiltrated with PL silane probe molecule 6 - higher magnification

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Figure 2b - raw data.lsm

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CLSM image of silica inverse opal infiltrated with PL silane probe molecule 6 - raw data- higher magnification

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Figure 3 - CLSM image of mesoporous silica.png

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CLSM image of mesoporous silica infiltrated with PL silane probe molecule 6

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elemental analysis - SiO2 + SAM.pdf

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Elemental analysis of bulk silica inverse opal immobilized with 3-azidopropyl triethoxysilane

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Figure 1a - Silica inverse opal-top view.tif

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SEM image of silica inverse opal

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Figure 1b - Silica inverse opal-cross secction.tif

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Cross section SEM image of silica inverse opal

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Figure 4a - Cross-section of bulk silica inverse opal.tif

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Cross-section SEM image of bulk silica inverse opal with inverse opal domains and mesoporous domains

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Figure 4b - Cross-section of bulk silica inverse opal.tif

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Cros-section SEM image presenting the border between an inverse opal domain and a mesoporous domain

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Figure S1a.tif

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SEM images of Si-IO-L1after immobilization of chiral diene-ligand L1 - lower magnification

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Figure S1b.tif

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SEM images of Si-IO-L1 after immobilization of chiral diene-ligand L1 - highe magnification

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Figure S1c.tif

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SEM images of Si-IO-L1 after immobilization of chiral diene-ligand L1 and 1st catalytic reaction - lower magnification

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Figure S1d.tif

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SEM images of Si-IO-L1 after immobilization of chiral diene-ligand L1 and 1st catalytic reaction - higher magnification

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Figure S1e.tif

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SEM images of Si-IO-L1 after immobilization of chiral diene-ligand L1 and 5st catalytic reaction - lower magnification

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Figure S1f.tif

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SEM images of Si-IO-L1 after immobilization of chiral diene-ligand L1 and 5st catalytic reaction - higher magnification

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