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Part 1: Document Description
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Citation |
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Title: |
Data for: Influence of the Synthesis Protocol on the Catalytic Performance of PHI-Type Zeolites for the Dehydration of Lactic Acid |
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Identification Number: |
doi:10.18419/darus-3338 |
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Distributor: |
DaRUS |
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Date of Distribution: |
2023-02-07 |
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Version: |
1 |
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Bibliographic Citation: |
Häussermann, Dorothea, 2023, "Data for: Influence of the Synthesis Protocol on the Catalytic Performance of PHI-Type Zeolites for the Dehydration of Lactic Acid", https://doi.org/10.18419/darus-3338, DaRUS, V1 |
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Citation |
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Title: |
Data for: Influence of the Synthesis Protocol on the Catalytic Performance of PHI-Type Zeolites for the Dehydration of Lactic Acid |
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Identification Number: |
doi:10.18419/darus-3338 |
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Authoring Entity: |
Häussermann, Dorothea (Universität Stuttgart) |
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Software used in Production: |
ASiQwin |
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Software used in Production: |
TopSpin |
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Software used in Production: |
Adobe Photoshop |
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Software used in Production: |
Agilent Chemstation |
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Software used in Production: |
ChemDraw |
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Grant Number: |
388060787 |
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Distributor: |
DaRUS |
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Access Authority: |
Häussermann, Dorothea |
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Access Authority: |
Traa, Yvonne |
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Depositor: |
Häussermann, Dorothea |
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Date of Deposit: |
2023-01-31 |
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Holdings Information: |
https://doi.org/10.18419/darus-3338 |
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Study Scope |
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Keywords: |
Chemistry, Zeolite Synthesis, Lactic Acid Dehydration, Acrylic Acid, Phillipsite |
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Topic Classification: |
Zeolites, Heterogeneous Catalysis |
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Abstract: |
<p>This dataset encludes all gas chromatography (GC), <sup>27</sup>Al magic angle spinning nuclear magnetic resonance spectroscopy (<sup>27</sup>Al MAS NMR), x-ray diffraction (XRD), CO<sub>2</sub> physisorption, inductively coupled plasma optical emission spectroscopy (ICP-OES) data and scanning electron microscope (SEM) images of the related publication: "Influence of the Synthesis Protocol on the Catalytic Performance of PHI-Type Zeolites for the Dehydration of Lactic Acid".</p> <p>The manuscript describes the influence of the synthesis protocol on the catalytic performance of PHI-type zeolites for the dehydration of lactic acid. Two PHI-type zeolites were synthesized with a few variations in the synthesis procedure. The catalysts were characterized and tested in the lactic acid dehydration reaction. During the catalytic reaction, a big difference in the performance was observed.</p> <p>The data used for the manuscript are sorted by the respective characterization method. The data are named according to the sample names. The raw data can be processed with the corresponding software.</p> |
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Methodology and Processing |
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Sources Statement |
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Data Access |
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Other Study Description Materials |
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Related Publications |
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Citation |
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Title: |
Häussermann, D.; Schömig, R.; Gehring, B.; Traa, Y. Influence of the Synthesis Protocol on the Catalytic Performance of PHI-Type Zeolites for the Dehydration of Lactic Acid. Catalysts 2023, 13, 261. |
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Identification Number: |
10.3390/catal13020261 |
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Bibliographic Citation: |
Häussermann, D.; Schömig, R.; Gehring, B.; Traa, Y. Influence of the Synthesis Protocol on the Catalytic Performance of PHI-Type Zeolites for the Dehydration of Lactic Acid. Catalysts 2023, 13, 261. |
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Label: |
GC_Na,K-PHI_hs_a.s._90%.zip |
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Text: |
GC data for Na,K-PHI_hs_a.s._90% |
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Notes: |
application/zip |
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Label: |
GC_Na,K-PHI_hs_calc_16.zip |
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Text: |
GC data forNa,K-PHI_hs_calc_16 |
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Notes: |
application/zip |
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Label: |
GC_Na,K-PHI_ls_calc_15%_a.zip |
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Text: |
GC data for Na,K-PHI_ls_calc_15% |
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Notes: |
application/zip |
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Label: |
GC_Na,K-PHI_ls_calc_15%_b.zip |
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Text: |
GC data for Na,K-PHI_ls_calc_15% |
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Notes: |
application/zip |
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Label: |
GC_Na,K-PHI_ls_calc_steamed_14%.zip |
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Text: |
GC data for Na,K-PHI_ls_calc_steamed_14% |
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Notes: |
application/zip |
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Label: |
Na,K-PHI_hs_a.s._90_10ym.tif |
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Text: |
SEM Image of Na,K-PHI_hs_a.s._90% |
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Notes: |
image/tiff |
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Label: |
Na,K-PHI_hs_a.s._90_1ym.tif |
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Text: |
SEM Image of Na,K-PHI_hs_a.s._90% |
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Notes: |
image/tiff |
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Label: |
Na,K-PHI_hs_calc_16_10ym.tif |
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Text: |
SEM Image of Na,K-PHI_hs_calc_16% |
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Notes: |
image/tiff |
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Label: |
Na,K-PHI_hs_calc_16_1ym.tif |
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Text: |
SEM Image of Na,K-PHI_hs_calc_16% |
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Notes: |
image/tiff |
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Label: |
Na,K-PHI_ls_calc_15_10ym.tif |
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Text: |
SEM Image of Na,K-PHI_ls_calc_15% |
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Notes: |
image/tiff |
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Label: |
Na,K-PHI_ls_calc_15_1ym.tif |
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Text: |
SEM Image of Na,K-PHI_ls_calc_15% |
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Notes: |
image/tiff |
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Label: |
PHI_27Al-MAS-NMR.xlsx |
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Text: |
collection of all 27 Al MAS NMR Data |
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Notes: |
application/vnd.openxmlformats-officedocument.spreadsheetml.sheet |
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Label: |
PHI_27Al-MAS-NMR_Na,K-PHI_hs_a.s._90%.zip |
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Text: |
27Al MAS NMR data for Na,K-PHI_hs_a.s._90% |
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Notes: |
application/zip |
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Label: |
PHI_27Al-MAS-NMR_Na,K-PHI_hs_a.s._N2_39%.zip |
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Text: |
27Al MAS NMR data for Na,K-PHI_hs_a.s._N2_39% |
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Notes: |
application/zip |
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Label: |
PHI_27Al-MAS-NMR_Na,K-PHI_hs_calc_16%.zip |
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Text: |
27Al MAS NMR data for Na,K-PHI_hs_calc_16% |
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Notes: |
application/zip |
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Label: |
PHI_27Al-MAS-NMR_Na,K-PHI_ls_calc_15%.zip |
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Text: |
27Al MAS NMR data for Na,K-PHI_ls_calc_15% |
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Notes: |
application/zip |
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Label: |
PHI_27Al-MAS-NMR_Na,K-PHI_ls_calc_steamed_14%.zip |
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Text: |
27Al MAS NMR data for Na,K-PHI_ls_calc_steamed_14% |
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Notes: |
application/zip |
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Label: |
PHI_catalysis_all.xlsx |
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Text: |
collection of catalysis data |
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Notes: |
application/vnd.openxmlformats-officedocument.spreadsheetml.sheet |
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Label: |
PHI_ICP.xlsx |
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Text: |
Raw Data of ICP-Data |
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Notes: |
application/vnd.openxmlformats-officedocument.spreadsheetml.sheet |
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Label: |
PHI_Physisorption_CO2.xlsx |
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Text: |
Collection of all CO2-Physisorption-data |
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Notes: |
application/vnd.openxmlformats-officedocument.spreadsheetml.sheet |
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Label: |
PHI_Physi_Na,K-PHI_hs_a.s._90%.pdf |
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Text: |
CO2-Physisorption of Na,K-PHI_hs_a.s._90% |
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Notes: |
application/pdf |
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Label: |
PHI_Physi_Na,K-PHI_hs_calc_16%.pdf |
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Text: |
CO2-Physisorption of Na,K-PHI_hs_calc_16% |
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Notes: |
application/pdf |
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Label: |
PHI_Physi_Na,K-PHI_ls_calc_15.pdf |
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Text: |
CO2-Physisorption of Na,K-PHI_ls_calc_15% |
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Notes: |
application/pdf |
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Label: |
PHI_XRD.xlsx |
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Text: |
collection of all XRD-data |
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Notes: |
application/vnd.openxmlformats-officedocument.spreadsheetml.sheet |
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Label: |
PHI_XRD_Raw_Na,K-PHI_hs_a.s._90.UXD |
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Text: |
XRD-raw-data of Na,K-PHI_hs_a.s._90% |
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Notes: |
application/octet-stream |
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Label: |
PHI_XRD_Raw_Na,K-PHI_hs_a.s._N2_39.UXD |
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Text: |
XRD-raw-data of Na,K-PHI_hs_a.s._N2_39% |
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Notes: |
application/octet-stream |
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Label: |
PHI_XRD_Raw_Na,K-PHI_hs_calc_16.UXD |
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Text: |
XRD-raw-data of Na,K-PHI_hs_calc_16% |
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Notes: |
application/octet-stream |
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Label: |
PHI_XRD_Raw_Na,K-PHI_ls_a.s._100.UXD |
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Text: |
XRD-raw-data of Na,K-PHI_ls_a.s._100% |
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Notes: |
application/octet-stream |
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Label: |
PHI_XRD_Raw_Na,K-PHI_ls_calc_15.UXD |
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Text: |
XRD-raw-data of Na,K-PHI_ls_calc_15% |
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Notes: |
application/octet-stream |
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Label: |
PHI_XRD_Raw_Na,K-PHI_ls_calc_steamed_14.UXD |
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Text: |
XRD-raw-data of Na,K-PHI_ls_calc_steamed_14% |
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Notes: |
application/octet-stream |
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Label: |
PHI_XRD_Raw_Na,K-PHI_ls_N2_15.UXD |
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Text: |
XRD-raw-data of Na,K-PHI_ls_N2_15% |
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Notes: |
application/octet-stream |