micro-XRCT data sets and in situ measured ultrasonic wave propagation of pre-stressed monodisperse rubber and glass particle mixtures with 10%, 20%, and 30% volume rubber content: samples 2 and 3 (doi:10.18419/darus-3437)

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Part 2: Study Description
Part 3: Data Files Description
Part 4: Variable Description
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micro-XRCT data sets and in situ measured ultrasonic wave propagation of pre-stressed monodisperse rubber and glass particle mixtures with 10%, 20%, and 30% volume rubber content: samples 2 and 3

doi:10.18419/darus-3437

DaRUS

2023-05-04

1

Ruf, Matthias; Taghizadeh, Kianoosh; Steeb, Holger, 2023, "micro-XRCT data sets and in situ measured ultrasonic wave propagation of pre-stressed monodisperse rubber and glass particle mixtures with 10%, 20%, and 30% volume rubber content: samples 2 and 3", https://doi.org/10.18419/darus-3437, DaRUS, V1, UNF:6:LyvQPm+lMHvJ9Z4neyxihA== [fileUNF]

micro-XRCT data sets and in situ measured ultrasonic wave propagation of pre-stressed monodisperse rubber and glass particle mixtures with 10%, 20%, and 30% volume rubber content: samples 2 and 3

doi:10.18419/darus-3437

Ruf, Matthias (University of Stuttgart, Institute of Applied Mechanics (CE))

Taghizadeh, Kianoosh (University of Stuttgart, Institute of Applied Mechanics (CE); University of Twente, Multiscale Mechanics (MSM))

Steeb, Holger (University of Stuttgart, Institute of Applied Mechanics (CE) & SC SimTech)

Ruf, Matthias

Taghizadeh, Kianoosh

Steeb, Holger

University of Stuttgart, Institute of Applied Mechanics (CE) - Chair for Continuum-Mechanics

University of Stuttgart - Cluster of Excellence EXC 2075 "SimTech"

2023

357361983

424876160

327154368

DaRUS

Steeb, Holger

https://doi.org/10.18419/darus-3437

Computer and Information Science, Earth and Environmental Sciences, Engineering, Physics, Granular Media, Granular Material, Wave Propagation, Micro X-Ray Computed Tomography (micro-XRCT), X-Ray Microtomography, Porous Media, Porous Medium, Geomechanics

This dataset contains 12 micro X-ray Computed Tomography (micro-XRCT) data sets from scans of cylindrical particulate mixture samples (diameter 80 mm; unloaded height 80 mm) under different uniaxial compression loads. The samples consist of monodisperse stiff (glass) and soft (rubber) particle mixtures. Both particles have an identical diameter of 4 mm. The considered samples have a volume fraction of 10%, 20%, and 30% rubber particles. Two individual mixtures were investigated for each volume fraction. The scans were performed in a low X-ray absorbing transparent oedometer cell with an integrated pair of P-wave ultrasonic transducers to determine in situ the sample stiffness based on wave propagation velocity measurements. On both sides, the wave travels through a 10 mm long Poly (methyl methacrylate) (PMMA) pre-run and after-run section before and after the wave enters and leaves the sample. <br><br> The respectively prepared sample inside the oedometer cell was uniaxially compressed in axial direction in subsequent force increments from F_stat. = 200 N to F_stat. = 1000 N (force-controlled) using a Universal Testing Machine (UTM) integrated into the XRCT system. At each force level, the system was relaxed for some time at the defined force to compensate the creep behavior of the soft particles. Subsequently, ultrasonic wave propagation measurements were performed at five different load levels, F_stat. = {200, 400, 600, 800, 1000} N. micro-XRCT scans were acquired in situ at F_stat. = {400, 800} N. For this, it was switched from force-controlled to displacement-controlled to avoid creeping and an eventual movement of the particles during the imaging. <br><br> In this data set, the reconstructed 3d volumes ("mixture_nu*_F400N_reconstructed.tar.gz" and "mixture_nu*_F800N_reconstructed.tar.gz"), as well as the projection images ("mixture_nu*_F400N_projections.tar.gz" and "mixture_nu*_F800N_projections.tar.gz") with * indicating the rubber volume fraction nu = {0.1, 0.2, 0.3} and the mixture counter {2, 3} for both preloads are given. For the datasets with counter "1" see the related datasets. The raw ultrasonic measurement data (transducer signals over time) is provided for all five preloads ("mixture_nu*_ultrasonic_data.tar.gz"), before and after the force-controlled relaxation, as an averaged signal of a stack of 32 signals. The file "mixture_nu*_utm_data.csv" contains the measured axial force and displacement from the UTM during the whole experiment. Based on the measured displacement of the UTM, the current mixture length was determined.

Image data

Numerical data (Measurement data)

Ruf, M. and Taghizadeh, K. contributed equally.

Taghizadeh, K. (2021). Raw data of wave propagation experiments using glass-rubber mixtures. 4TU.ResearchData. <a href="https://doi.org/10.4121/14096491.v1">https://doi.org/10.4121/14096491.v1</a>

<br>Ruf, M., Taghizadeh, K. & Steeb, H. (2021). micro-XRCT data sets and in situ measured ultrasonic wave propagation of a pre-stressed monodisperse rubber and glass particle mixture with 50% volume rubber content. DaRUS. <a href="https://doi.org/10.18419/darus-2208">https://doi.org/10.18419/darus-2208</a>

<br>Ruf, M., Taghizadeh, K. & Steeb, H. (2022). micro-XRCT data sets and in situ measured ultrasonic wave propagation of a pre-stressed monodisperse rubber and glass particle mixture with 30% volume rubber content. DaRUS. <a href="https://doi.org/10.18419/darus-2833">https://doi.org/10.18419/darus-2833</a>

<br>Ruf, M., Taghizadeh, K. & Steeb, H. (2023). micro-XRCT data sets and in situ measured ultrasonic wave propagation of pre-stressed monodisperse rubber and glass particle mixtures with 10%, 20%, 40%, and 60% volume rubber content: sample 1. DaRUS. <a href="https://doi.org/10.18419/darus-3436">https://doi.org/10.18419/darus-3436</a>

Taghizadeh, K., Ruf, M., Luding, S., & Steeb, H. (2023). X-ray 3D imaging–based microunderstanding of granular mixtures: Stiffness enhancement by adding small fractions of soft particles. <em>Proceedings of the National Academy of Sciences</em>, 120(26), e2219999120.

10.1073/pnas.2219999120

Taghizadeh, K., Ruf, M., Luding, S., & Steeb, H. (2023). X-ray 3D imaging–based microunderstanding of granular mixtures: Stiffness enhancement by adding small fractions of soft particles. <em>Proceedings of the National Academy of Sciences</em>, 120(26), e2219999120.

Ruf, M., Taghizadeh, K. & Steeb, H. (2022). Multi-scale characterization of granular media by in situ laboratory X-ray computed tomography. <em>GAMM Mitteilungen</em>, 45(3-4), e202200011.

10.1002/gamm.202200011

Ruf, M., Taghizadeh, K. & Steeb, H. (2022). Multi-scale characterization of granular media by in situ laboratory X-ray computed tomography. <em>GAMM Mitteilungen</em>, 45(3-4), e202200011.

Ruf, M., & Steeb, H. (2020). An open, modular, and flexible micro X-ray computed tomography system for research. <em>Review of Scientific Instruments</em>, 91(11), 113102. <a href="https://doi.org/10.1063/5.0019541">https://doi.org/10.1063/5.0019541</a>

<br>Taghizadeh, K., Steeb, H., Luding, S., & Magnanimo, V. (2021). Elastic waves in particulate glass-rubber mixtures. <em>Proceedings of the Royal Society A</em>, 477(2249), 20200834, <a href="https://doi.org/10.1098/rspa.2020.0834">https://doi.org/10.1098/rspa.2020.0834</a>

• Number of cases: 1344866

• No. of variables per record: 3

• Type of File: text/tab-separated-values

UNF:6:J8grVS9/d/mdy1bLiglYEg==

• Number of cases: 1332831

• No. of variables per record: 3

• Type of File: text/tab-separated-values

UNF:6:H+dbbglohkkVmtzd1AZLwA==

• Number of cases: 1362768

• No. of variables per record: 3

• Type of File: text/tab-separated-values

UNF:6:IRTwG69rDWkHefHtGGdsFA==

• Number of cases: 1312785

• No. of variables per record: 3

• Type of File: text/tab-separated-values

UNF:6:sQwWC0+eCpWETZ9ES+SW6g==

• Number of cases: 1453485

• No. of variables per record: 3

• Type of File: text/tab-separated-values

UNF:6:uoD560iPYVJEm7ln8IYgPA==

• Number of cases: 1331554

• No. of variables per record: 3

• Type of File: text/tab-separated-values

UNF:6:PqJh05I1T9bb+Z0XmMl2ZQ==

• time [s] - time [s]
• displacement [mm] - displacement [mm]
• force [N] - force [N]
• time [s] - time [s]
• displacement [mm] - displacement [mm]
• force [N] - force [N]
• time [s] - time [s]
• displacement [mm] - displacement [mm]
• force [N] - force [N]
• time [s] - time [s]
• displacement [mm] - displacement [mm]
• force [N] - force [N]
• time [s] - time [s]
• displacement [mm] - displacement [mm]
• force [N] - force [N]
• time [s] - time [s]
• displacement [mm] - displacement [mm]
• force [N] - force [N]

f201504 Location:

Summary Statistics: Mean 13448.669999972028; Max. 26897.3203; Min. 0.02; Valid 1344866.0; StDev 7764.590357990671

Variable Format: numeric

Notes: UNF:6:bruHgKi81ZElhtahFfPtLQ==

f201504 Location:

Summary Statistics: Max. 2.0646; Mean 1.6031818933625366; Min. 3.0E-4; Valid 1344866.0; StDev 0.2504085779995828

Variable Format: numeric

Notes: UNF:6:M6j+1KWX8+lW3ENv8Jow7w==

f201504 Location:

Summary Statistics: Mean 412.266079572181; Min. 1.835; Valid 1344866.0; Max. 1000.265; StDev 215.28585824103988

Variable Format: numeric

Notes: UNF:6:vsGgDjzOdFDs8xYCW+b61Q==

f201503 Location:

Summary Statistics: Max. 26656.6191; Min. 0.02; StDev 7695.106253092924; Valid 1332831.0; Mean 13328.320000027323;

Variable Format: numeric

Notes: UNF:6:qmINdXhzrstPdv+THlop1w==

f201503 Location:

Summary Statistics: Max. 2.098; StDev 0.24272751583504953; Valid 1332831.0; Mean 1.6966893010458293; Min. -0.0;

Variable Format: numeric

Notes: UNF:6:sUa78OrsnAbrvs3TuG5ybg==

f201503 Location:

Summary Statistics: Valid 1332831.0; StDev 209.68883051237862; Mean 435.9083927895565; Max. 1000.265; Min. 1.835;

Variable Format: numeric

Notes: UNF:6:cG2Q1ihWENW4BW00Rz+stw==

f201501 Location:

Summary Statistics: Valid 1362768.0; Max. 27255.3594; StDev 7867.947603179426; Min. 0.02; Mean 13627.690000004359

Variable Format: numeric

Notes: UNF:6:qAE5sy053XrfmA6FCyimYw==

f201501 Location:

Summary Statistics: Max. 3.8134; Valid 1362768.0; Mean 2.878234237450949; StDev 0.5515714045333165; Min. -0.0;

Variable Format: numeric

Notes: UNF:6:Cl4S0yLlZN/5lJQkzQSxPg==

f201501 Location:

Summary Statistics: Max. 1000.185; Min. 1.775; Mean 460.7905000008385; StDev 190.73537202700118; Valid 1362768.0

Variable Format: numeric

Notes: UNF:6:h6WCLHouKQe/3ynm6Uqjew==

f201502 Location:

Summary Statistics: Min. 0.02; StDev 7579.370618130187; Max. 26255.6992; Valid 1312785.0; Mean 13127.85999998754

Variable Format: numeric

Notes: UNF:6:hQCHj16r6Ww+qnPJEqu/5Q==

f201502 Location:

Summary Statistics: Min. -0.0; Mean 3.6535096532969766; Max. 4.5554; StDev 0.5610343954720414; Valid 1312785.0;

Variable Format: numeric

Notes: UNF:6:Yd866tW3tqnqaeffoYRVLQ==

f201502 Location:

Summary Statistics: Min. 1.775; Mean 468.1422245684409; StDev 193.45882008455766; Max. 1000.3; Valid 1312785.0

Variable Format: numeric

Notes: UNF:6:djuDZGNcuRZ5eiI+tbkAlw==

f201500 Location:

Summary Statistics: Min. 0.02; StDev 8391.702446880838; Mean 14534.860000041708; Max. 29069.6992; Valid 1453485.0

Variable Format: numeric

Notes: UNF:6:1UjhapQWtB2CqX/5lgLhKw==

f201500 Location:

Summary Statistics: Max. 6.9806; Mean 5.379983698079881; Valid 1453485.0; StDev 0.9728097045679617; Min. -0.0

Variable Format: numeric

Notes: UNF:6:6kTEtr/8ViKjLu9p3rQ5/g==

f201500 Location:

Summary Statistics: Valid 1453485.0; Max. 1000.185; Mean 489.6253190709662; Min. 1.37; StDev 200.33066304673332

Variable Format: numeric

Notes: UNF:6:6P2L9kQxvXxNzAlw6JzDPw==

f201505 Location:

Summary Statistics: Valid 1331554.0; StDev 7687.733490156896; Min. 0.02; Mean 13315.549999956578; Max. 26631.0801

Variable Format: numeric

Notes: UNF:6:0RpGFxjg7/Mu5LIMToxicg==

f201505 Location:

Summary Statistics: StDev 0.9500215494562516; Valid 1331554.0; Min. -0.0; Max. 7.2436; Mean 5.721908481594589;

Variable Format: numeric

Notes: UNF:6:X+Js37QJXKiMDjnbuasfXw==

f201505 Location:

Summary Statistics: Max. 1000.24; Mean 488.6250599186548; Min. 1.775; Valid 1331554.0; StDev 195.68897722186415;

Variable Format: numeric

Notes: UNF:6:SS/bwbTZIKYJJ3dOdpw3KA==

Label:

mixture_nu0.1-2_F400N_projections.tar.gz

Text:

Projection images (360 deg, angle increment 0.25 deg), dark image (di), and open beam image (ob) in 16 bit *.tif file format. Volume percent rubber particles nu = 10%, sample 2, preload F_stat. = 400 N.

application/x-gzip

Label:

mixture_nu0.1-2_F400N_reconstructed.tar.gz

Text:

Reconstructed micro-XRCT data set in 16 bit *.tif file format. 972x972x768 voxels with the uniform voxel size of 110 µm. Volume percent rubber particles nu = 10%, sample 2, preload F_stat. = 400 N.

application/x-gzip

Label:

mixture_nu0.1-2_F800N_projections.tar.gz

Text:

Projection images (360 deg, angle increment 0.25 deg), dark image (di), and open beam image (ob) in 16 bit *.tif file format. Volume percent rubber particles nu = 10%, sample 2, preload F_stat. = 800 N.

application/x-gzip

Label:

mixture_nu0.1-2_F800N_reconstructed.tar.gz

Text:

Reconstructed micro-XRCT data set in 16 bit *.tif file format. 972x972x768 voxels with the uniform voxel size of 110 µm. Volume percent rubber particles nu = 10%, sample 2, preload F_stat. = 800 N.

application/x-gzip

Label:

mixture_nu0.1-2_ultrasonic_data.tar.gz

Text:

Raw ultrasonic measurement data in *.psdata and *.csv file format. Volume percent rubber particles nu = 10%, sample 2. File name schema: rubber volume fraction of the mixture ("nu"); static preload F_stat. in N ("F"); measurement date. Oscilloscope channels: A = receiver transducer signal; B = transmitter transducer signal.

application/x-gzip

Label:

mixture_nu0.1-3_F400N_projections.tar.gz

Text:

Projection images (360 deg, angle increment 0.25 deg), dark image (di), and open beam image (ob) in 16 bit *.tif file format. Volume percent rubber particles nu = 10%, sample 3, preload F_stat. = 400 N.

application/x-gzip

Label:

mixture_nu0.1-3_F400N_reconstructed.tar.gz

Text:

Reconstructed micro-XRCT data set in 16 bit *.tif file format. 972x972x768 voxels with the uniform voxel size of 110 µm. Volume percent rubber particles nu = 10%, sample 3, preload F_stat. = 400 N.

application/x-gzip

Label:

mixture_nu0.1-3_F800N_projections.tar.gz

Text:

Projection images (360 deg, angle increment 0.25 deg), dark image (di), and open beam image (ob) in 16 bit *.tif file format. Volume percent rubber particles nu = 10%, sample 3, preload F_stat. = 800 N.

application/x-gzip

Label:

mixture_nu0.1-3_F800N_reconstructed.tar.gz

Text:

Reconstructed micro-XRCT data set in 16 bit *.tif file format. 972x972x768 voxels with the uniform voxel size of 110 µm. Volume percent rubber particles nu = 10%, sample 3, preload F_stat. = 800 N.

application/x-gzip

Label:

mixture_nu0.1-3_ultrasonic_data.tar.gz

Text:

Raw ultrasonic measurement data in *.psdata and *.csv file format. Volume percent rubber particles nu = 10%, sample 3. File name schema: rubber volume fraction of the mixture ("nu"); static preload F_stat. in N ("F"); measurement date. Oscilloscope channels: A = receiver transducer signal; B = transmitter transducer signal.

application/x-gzip

Label:

mixture_nu0.2-2_F400N_projections.tar.gz

Text:

Projection images (360 deg, angle increment 0.25 deg), dark image (di), and open beam image (ob) in 16 bit *.tif file format. Volume percent rubber particles nu = 20%, sample 2, preload F_stat. = 400 N.

application/x-gzip

Label:

mixture_nu0.2-2_F400N_reconstructed.tar.gz

Text:

Reconstructed micro-XRCT data set in 16 bit *.tif file format. 972x972x768 voxels with the uniform voxel size of 110 µm. Volume percent rubber particles nu = 20%, sample 2, preload F_stat. = 400 N.

application/x-gzip

Label:

mixture_nu0.2-2_F800N_projections.tar.gz

Text:

Projection images (360 deg, angle increment 0.25 deg), dark image (di), and open beam image (ob) in 16 bit *.tif file format. Volume percent rubber particles nu = 20%, sample 2, preload F_stat. = 800 N.

application/x-gzip

Label:

mixture_nu0.2-2_F800N_reconstructed.tar.gz

Text:

Reconstructed micro-XRCT data set in 16 bit *.tif file format. 972x972x768 voxels with the uniform voxel size of 110 µm. Volume percent rubber particles nu = 20%, sample 2, preload F_stat. = 800 N.

application/x-gzip

Label:

mixture_nu0.2-2_ultrasonic_data.tar.gz

Text:

Raw ultrasonic measurement data in *.psdata and *.csv file format. Volume percent rubber particles nu = 20%, sample 2. File name schema: rubber volume fraction of the mixture ("nu"); static preload F_stat. in N ("F"); measurement date. Oscilloscope channels: A = receiver transducer signal; B = transmitter transducer signal.

application/x-gzip

Label:

mixture_nu0.2-3_F400N_projections.tar.gz

Text:

Projection images (360 deg, angle increment 0.25 deg), dark image (di), and open beam image (ob) in 16 bit *.tif file format. Volume percent rubber particles nu = 20%, sample 3, preload F_stat. = 800 N.

application/x-gzip

Label:

mixture_nu0.2-3_F400N_reconstructed.tar.gz

Text:

Reconstructed micro-XRCT data set in 16 bit *.tif file format. 972x972x768 voxels with the uniform voxel size of 110 µm. Volume percent rubber particles nu = 20%, sample 3, preload F_stat. = 400 N.

application/x-gzip

Label:

mixture_nu0.2-3_F800N_projections.tar.gz

Text:

Projection images (360 deg, angle increment 0.25 deg), dark image (di), and open beam image (ob) in 16 bit *.tif file format. Volume percent rubber particles nu = 20%, sample 3, preload F_stat. = 400 N.

application/x-gzip

Label:

mixture_nu0.2-3_F800N_reconstructed.tar.gz

Text:

Reconstructed micro-XRCT data set in 16 bit *.tif file format. 972x972x768 voxels with the uniform voxel size of 110 µm. Volume percent rubber particles nu = 20%, sample 3, preload F_stat. = 800 N.

application/x-gzip

Label:

mixture_nu0.2-3_ultrasonic_data.tar.gz

Text:

Raw ultrasonic measurement data in *.psdata and *.csv file format. Volume percent rubber particles nu = 20%, sample 3. File name schema: rubber volume fraction of the mixture ("nu"); static preload F_stat. in N ("F"); measurement date. Oscilloscope channels: A = receiver transducer signal; B = transmitter transducer signal.

application/x-gzip

Label:

mixture_nu0.3-2_F400N_projections.tar.gz

Text:

Projection images (360 deg, angle increment 0.25 deg), dark image (di), and open beam image (ob) in 16 bit *.tif file format. Volume percent rubber particles nu = 30%, sample 2, preload F_stat. = 400 N.

application/x-gzip

Label:

mixture_nu0.3-2_F400N_reconstructed.tar.gz

Text:

Reconstructed micro-XRCT data set in 16 bit *.tif file format. 972x972x768 voxels with the uniform voxel size of 110 µm. Volume percent rubber particles nu = 30%, sample 2, preload F_stat. = 400 N.

application/x-gzip

Label:

mixture_nu0.3-2_F800N_projections.tar.gz

Text:

Projection images (360 deg, angle increment 0.25 deg), dark image (di), and open beam image (ob) in 16 bit *.tif file format. Volume percent rubber particles nu = 30%, sample 2, preload F_stat. = 800 N.

application/x-gzip

Label:

mixture_nu0.3-2_F800N_reconstructed.tar.gz

Text:

Reconstructed micro-XRCT data set in 16 bit *.tif file format. 972x972x768 voxels with the uniform voxel size of 110 µm. Volume percent rubber particles nu = 30%, sample 2, preload F_stat. = 800 N.

application/x-gzip

Label:

mixture_nu0.3-2_ultrasonic_data.tar.gz

Text:

Raw ultrasonic measurement data in *.psdata and *.csv file format. Volume percent rubber particles nu = 30%, sample 2. File name schema: rubber volume fraction of the mixture ("nu"); static preload F_stat. in N ("F"); measurement date. Oscilloscope channels: A = receiver transducer signal; B = transmitter transducer signal.

application/x-gzip

Label:

mixture_nu0.3-3_F400N_projections.tar.gz

Text:

Projection images (360 deg, angle increment 0.25 deg), dark image (di), and open beam image (ob) in 16 bit *.tif file format. Volume percent rubber particles nu = 30%, sample 3, preload F_stat. = 400 N.

application/x-gzip

Label:

mixture_nu0.3-3_F400N_reconstructed.tar.gz

Text:

Reconstructed micro-XRCT data set in 16 bit *.tif file format. 972x972x768 voxels with the uniform voxel size of 110 µm. Volume percent rubber particles nu = 30%, sample 3, preload F_stat. = 400 N.

application/x-gzip

Label:

mixture_nu0.3-3_F800N_projections.tar.gz

Text:

Projection images (360 deg, angle increment 0.25 deg), dark image (di), and open beam image (ob) in 16 bit *.tif file format. Volume percent rubber particles nu = 30%, sample 3, preload F_stat. = 800 N.

application/x-gzip

Label:

mixture_nu0.3-3_F800N_reconstructed.tar.gz

Text:

Reconstructed micro-XRCT data set in 16 bit *.tif file format. 972x972x768 voxels with the uniform voxel size of 110 µm. Volume percent rubber particles nu = 30%, sample 3, preload F_stat. = 800 N.

application/x-gzip

Label:

mixture_nu0.3-3_ultrasonic_data.tar.gz

Text:

Raw ultrasonic measurement data in *.psdata and *.csv file format. Volume percent rubber particles nu = 30%, sample 3. File name schema: rubber volume fraction of the mixture ("nu"); static preload F_stat. in N ("F"); measurement date. Oscilloscope channels: A = receiver transducer signal; B = transmitter transducer signal.

application/x-gzip