Data for: Rheological Analysis and Evaluation of Measurement Techniques for the Curing Polymethylmethacrylate Bone Cement in Vertebroplasty (doi:10.18419/darus-4004)

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Part 1: Document Description
Part 2: Study Description
Part 3: Data Files Description
Part 4: Variable Description
Part 5: Other Study-Related Materials
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Data for: Rheological Analysis and Evaluation of Measurement Techniques for the Curing Polymethylmethacrylate Bone Cement in Vertebroplasty

doi:10.18419/darus-4004

DaRUS

2024-05-15

1

Trivedi, Zubin; Wychowaniec, Jacek K.; Gehweiler, Dominic; Sprecher, Christoph Martin; Boger, Andreas; Gueorguiev, Boyko; D'Este, Matteo; Ricken, Tim; Röhrle, Oliver, 2024, "Data for: Rheological Analysis and Evaluation of Measurement Techniques for the Curing Polymethylmethacrylate Bone Cement in Vertebroplasty", https://doi.org/10.18419/darus-4004, DaRUS, V1, UNF:6:qWipgRgsaAlTQZDkmPv0LQ== [fileUNF]

Data for: Rheological Analysis and Evaluation of Measurement Techniques for the Curing Polymethylmethacrylate Bone Cement in Vertebroplasty

doi:10.18419/darus-4004

Trivedi, Zubin (University of Stuttgart)

Wychowaniec, Jacek K. (AO Research Institute Davos)

Gehweiler, Dominic (AO Research Institute Davos)

Sprecher, Christoph Martin (AO Research Institute Davos)

Boger, Andreas (Ansbach University of Applied Sciences)

Gueorguiev, Boyko (AO Research Institute Davos)

D'Este, Matteo (AO Research Institute Davos)

Ricken, Tim (University of Stuttgart)

Röhrle, Oliver (University of Stuttgart)

327154368 - SFB 1313

DaRUS

Trivedi, Zubin

Trivedi, Zubin

Trivedi, Zubin

2024-02-16

https://doi.org/10.18419/darus-4004

Engineering, Medicine, Health and Life Sciences, Vertebroplasty, Bone Cements, Non-Newtonian, Non-Newtonian Fluids, Rheology, Viscoelasticity, PMMA

<p>This dataset includes the measurement data described in the paper &quot;Rheological Analysis and Evaluation of Measurement Techniques for the Curing Polymethylmethacrylate Bone Cement in Vertebroplasty&quot; and additional supplementary data. All data in .csv files except 'Inj1 -- 5' are generated directly by the rheometer software from the rheometer measurements. </p> <p>Microsoft Excel files:</p> <ul> <li>settings.xlsx: Contains settings for all the measurements</li> </ul> <p>Comma separated value files:</p> <ul> <li>Benchmark-1 -- 4.csv: Oscillatory test at 3 mNm torque amplitude and 1 Hz frequency (Fig.S1)</li> <li> <p>Inj1 -- 5.csv: Injection test at 0.025 mL/s (Fig. 7a, 7b)</p> </li> <li> <p>Rh1a.csv: Oscillatory deformation of 0.2\% strain amplitude and 1 Hz frequency for 30 minutes (Fig. 2a)</p> </li> <li> <p>Rh1b.csv: Oscillatory deformation of 20\% strain amplitude and 1 Hz frequency for 30 minutes (Fig. 2b)</p> </li> <li> <p>Rh2a.csv: Oscillatory deformation in three stages: (i) 0.1\% strain amplitude, 0.1 Hz (5 mins) (ii) 20\% strain amplitude, 1 Hz (3 mins) (iii) 0.1\% strain amplitude, 0.1 Hz (22 mins) (Fig. 2c)</p> </li> <li> <p>Rh2b.csv: Oscillatory deformation in three stages: (i) 0.1\% strain amplitude, 0.1 Hz, 23 &deg;C (5 mins) (ii) 20\% strain amplitude, 1 Hz, 23 &deg;C (3 mins) (iii) 0.1\% strain amplitude, 0.1 Hz, 37 &deg;C (22 mins) (Fig. 2d)</p> </li> <li> <p>Rh3.csv: Rotational shear stress was applied in steps of (i) 0 Pa (ii) 100 Pa (iii) 0 Pa (iv) 500 Pa (v) 0 Pa (vi) 2000 Pa (vii) 0 Pa, of one minute each, to evaluate creep behaviour. (Fig. 3a)</p> </li> <li> <p>Rh4-1.csv: Rotational shear strain was applied in steps of (i) 0\% (ii) 1\% (iii) 0\%, of two minutes each. (Fig. 3b)</p> </li> <li> <p>Rh4-2.csv: Rotational shear strain was applied in steps of (i) 0\% (ii) 100\% (iii) 0\%, of two minutes each. (Fig. 3b)</p> </li> <li> <p>Rh5-1 -- 3.csv: Amplitude sweep test, where the strain amplitude was gradually increased from 0.01\% to 1000\%. The test was done at 1 Hz frequency (Fig. 3c, 3d)</p> </li> <li> <p>Rh6-1 -- 3.csv: Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.01% strain amplitude (Fig. 3e, 3f)</p> </li> <li> <p>Rh6-4 -- 6.csv: Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.03% strain amplitude (Fig. 5)</p> </li> <li> <p>Rh6-7 -- 9.csv: Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.2% strain amplitude (Fig. 5)</p> </li> <li> <p>Rh6-10.csv: Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 200% strain amplitude (Fig. 5)</p> </li> <li> <p>Rh7a-1.csv: Rotational shear rate sweep from 0.001 to 1000 1/s (Fig. 4a, 4b)</p> </li> <li> <p>Rh7a-2.csv: Rotational shear rate sweep from 0.01 to 1 1/s (Fig. 4a, 4b)</p> </li> <li> <p>Rh7a-3.csv: Rotational shear rate sweep from 0.001 to 0.01 1/s (Fig. 4a, 4b)</p> </li> <li> <p>Rh7a-4.csv: Rotational shear rate sweep from 1 to 100 1/s (Fig. 4a, 4b)</p> </li> <li> <p>Rh7a-5.csv: Rotational shear rate sweep from 10 to 1000 1/s (Fig. 4a, 4b)</p> </li> <li> <p>Rh7b-1.csv: Rotational shear rate sweep from 0.1 to 100 1/s with sandpaper (Fig. 4a, 4b)</p> </li> <li> <p>Rh7b-2.csv: Rotational shear rate sweep from 0.1 to 100 1/s with sandpaper (Fig. 4a, 4b)</p> </li> <li> <p>Rh7b-3.csv: Rotational shear rate sweep from 0.1 to 100 1/s with sandpaper (Fig. 4a, 4b)</p> </li> <li> <p>Rh8-1.csv: Constant rotational shear rate 0.0001 1/s for 20 minutes (Fig. 4c)</p> </li> <li> <p>Rh8-2.csv: Constant rotational shear rate 0.001 1/s for 20 minutes (Fig. 4c)</p> </li> <li> <p>Rh8-3.csv: Constant rotational shear rate 0.01 1/s for 20 minutes (Fig. 4c)</p> </li> <li> <p>Rh8-4.csv: Constant rotational shear rate 0.1 1/s for 20 minutes (Fig. 4c)</p> </li> <li> <p>Rh8-5.csv: Constant rotational shear rate 1 1/s for 20 minutes (Fig. 4c)</p> </li> <li> <p>Rh8-6.csv: Constant rotational shear rate 100 1/s for 20 minutes (Fig. 4c)</p> </li> <li> <p>Rh9.csv: Bone cement was prepared and simply left on the rheometer between the plates while maintaining 1.5 mm gap for 45 minutes without any action.</p> </li> <li> <p>Rh10.csv: Bone cement was prepared and subjected to 15 minutes of rotational 100 1/s shear rate and then 30 minutes of no action on the rheometer.</p> </li> </ul>

Trivedi, Z., Wychowaniec, J. K., Gehweiler, D., Sprecher, C. M., Boger, A., Gueorguiev, B., D’Este, M., Ricken, T., & Röhrle, O. (2023). Rheological Analysis and Evaluation of Measurement Techniques for the Curing Polymethylmethacrylate Bone Cement in Vertebroplasty.

arXiv:2312.11426

Trivedi, Z., Wychowaniec, J. K., Gehweiler, D., Sprecher, C. M., Boger, A., Gueorguiev, B., D’Este, M., Ricken, T., & Röhrle, O. (2023). Rheological Analysis and Evaluation of Measurement Techniques for the Curing Polymethylmethacrylate Bone Cement in Vertebroplasty.

• Number of cases: 1582

• No. of variables per record: 2

• Type of File: text/tab-separated-values

UNF:6:9FvbgiUvM5buhRa0GNwedg==

• Number of cases: 801

• No. of variables per record: 2

• Type of File: text/tab-separated-values

UNF:6:cQ5ceGSSFGO8pYiQF6aOlg==

• Number of cases: 410

• No. of variables per record: 2

• Type of File: text/tab-separated-values

UNF:6:ZzKVSTLgyvim0f/NBcdNrA==

• Number of cases: 215

• No. of variables per record: 2

• Type of File: text/tab-separated-values

UNF:6:JYYhuJ9dufRqnC+G5/wyqw==

• Number of cases: 117

• No. of variables per record: 2

• Type of File: text/tab-separated-values

UNF:6:yXUKoRIus24AzLU1n4Ho7w==

• Time [s] - Time [s]
• Force [N] - Force [N]
• Time [s]  - Time [s]
• Force [N] - Force [N]
• Time [s] - Time [s]
• Force [N] - Force [N]
• Time [s] - Time [s]
• Force [N] - Force [N]
• Time [s] - Time [s]
• Force [N] - Force [N]

f283627 Location:

Summary Statistics: Min. 0.05; Mean 39.575; Valid 1582.0; Max. 79.1; StDev 22.841418884707373;

Variable Format: numeric

Notes: UNF:6:bzN2h/eVEzhwVsNiqNcYkA==

f283627 Location:

Summary Statistics: Max. 19.72510351; StDev 2.0255995487969622; Mean 12.356950377722503; Valid 1582.0; Min. 3.218517948

Variable Format: numeric

Notes: UNF:6:Xv+6vaRuq1VIl7DG4bXHyQ==

f283619 Location:

Summary Statistics: StDev 11.568653767833144; Max. 40.05; Mean 20.05; Min. 0.05; Valid 801.0;

Variable Format: numeric

Notes: UNF:6:FyuiTPFqkl7jSyv9eR9mDQ==

f283619 Location:

Summary Statistics: Max. 25.25960191; Mean 18.283241194166045; Min. 2.736099673; StDev 3.5027376749995316; Valid 801.0;

Variable Format: numeric

Notes: UNF:6:dfc+8j0f+DD/G2YwjOQ27Q==

f283641 Location:

Summary Statistics: Min. 0.05; Valid 410.0; Mean 10.275; Max. 20.5; StDev 5.925052742381286

Variable Format: numeric

Notes: UNF:6:W47boXgzWsTQyws8sxbCNg==

f283641 Location:

Summary Statistics: Min. 2.940002185; Valid 410.0; StDev 4.330383473377027; Max. 23.06738716; Mean 20.624516392185367;

Variable Format: numeric

Notes: UNF:6:OAj+JDHFf5BoDGSIh+FIug==

f283638 Location:

Summary Statistics: Max. 10.75; Mean 5.400000000000001; Valid 215.0; Min. 0.05; StDev 3.110466202999158;

Variable Format: numeric

Notes: UNF:6:b9Gx8yI6hRVbGGbPjAEa+w==

f283638 Location:

Summary Statistics: Min. 2.365500202; StDev 7.1314781262684335; Mean 24.094259252832558; Max. 32.45008356; Valid 215.0

Variable Format: numeric

Notes: UNF:6:3dRKCEeG328LOwStRCMLbg==

f283617 Location:

Summary Statistics: Max. 5.85; Valid 117.0; Min. 0.05; StDev 1.6959510606146626; Mean 2.95

Variable Format: numeric

Notes: UNF:6:ocW3/cbrkWO8wXCTnq1CRA==

f283617 Location:

Summary Statistics: Min. 2.714268386; Valid 117.0; Max. 34.07678095; Mean 26.866584230666668; StDev 10.460409201292562

Variable Format: numeric

Notes: UNF:6:HVFYA/s5l08+5ZIxvxJSTw==

Label:

Benchmark-1.csv

Text:

Oscillatory test at 3 mNm torque amplitude and 1 Hz frequency (Fig.S1)

text/comma-separated-values

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Benchmark-2.csv

Text:

Oscillatory test at 3 mNm torque amplitude and 1 Hz frequency (Fig.S1)

text/comma-separated-values

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Benchmark-3.csv

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Oscillatory test at 3 mNm torque amplitude and 1 Hz frequency (Fig.S1)

text/comma-separated-values

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Benchmark-4.csv

Text:

Oscillatory test at 3 mNm torque amplitude and 1 Hz frequency (Fig.S1)

text/comma-separated-values

Label:

Rh10.csv

Text:

Bone cement was prepared and subjected to 15 minutes of rotational 100 1/s shear rate and then 30 minutes of no action on the rheometer.

text/comma-separated-values

Label:

Rh1a.csv

Text:

Oscillatory deformation of 0.2\% strain amplitude and 1 Hz frequency for 30 minutes (Fig. 2a)

text/comma-separated-values

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Rh1b.csv

Text:

Oscillatory deformation of 20\% strain amplitude and 1 Hz frequency for 30 minutes (Fig. 2b)

text/comma-separated-values

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Rh2a.csv

Text:

Oscillatory deformation in three stages: (i) 0.1\% strain amplitude, 0.1 Hz (5 mins) (ii) 20\% strain amplitude, 1 Hz (3 mins) (iii) 0.1\% strain amplitude, 0.1 Hz (22 mins) (Fig. 2c)

text/comma-separated-values

Label:

Rh2b.csv

Text:

Oscillatory deformation in three stages: (i) 0.1\% strain amplitude, 0.1 Hz, 23 °C (5 mins) (ii) 20\% strain amplitude, 1 Hz, 23 °C (3 mins) (iii) 0.1\% strain amplitude, 0.1 Hz, 37 °C (22 mins) (Fig. 2d)

text/csv

Label:

Rh3.csv

Text:

Rotational shear stress was applied in steps of (i) 0 Pa (ii) 100 Pa (iii) 0 Pa (iv) 500 Pa (v) 0 Pa (vi) 2000 Pa (vii) 0 Pa, of one minute each, to evaluate creep behaviour. (Fig. 3a)

text/comma-separated-values

Label:

Rh4-1.csv

Text:

Rotational shear strain was applied in steps of (i) 0\% (ii) 1\% (iii) 0\%, of two minutes each. (Fig. 3b)

text/comma-separated-values

Label:

Rh4-2.csv

Text:

Rotational shear strain was applied in steps of (i) 0\% (ii) 100\% (iii) 0\%, of two minutes each. (Fig. 3b)

text/comma-separated-values

Label:

Rh5-1.csv

Text:

Amplitude sweep test, where the strain amplitude was gradually increased from 0.01\% to 1000\%. The test was done at 1 Hz frequency (Fig. 3c, 3d)

text/comma-separated-values

Label:

Rh5-2.csv

Text:

Amplitude sweep test, where the strain amplitude was gradually increased from 0.01\% to 1000\%. The test was done at 1 Hz frequency (Fig. 3c, 3d)

text/comma-separated-values

Label:

Rh5-3.csv

Text:

Amplitude sweep test, where the strain amplitude was gradually increased from 0.01\% to 1000\%. The test was done at 1 Hz frequency (Fig. 3c, 3d)

text/comma-separated-values

Label:

Rh6-1.csv

Text:

Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.01% strain amplitude (Fig. 3e, 3f)

text/comma-separated-values

Label:

Rh6-10.csv

Text:

Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 200% strain amplitude (Fig. 5)

text/comma-separated-values

Label:

Rh6-2.csv

Text:

Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.01% strain amplitude (Fig. 3e, 3f)

text/comma-separated-values

Label:

Rh6-3.csv

Text:

Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.01% strain amplitude (Fig. 3e, 3f)

text/comma-separated-values

Label:

Rh6-4.csv

Text:

Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.03% strain amplitude (Fig. 5)

text/comma-separated-values

Label:

Rh6-5.csv

Text:

Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.03% strain amplitude (Fig. 5)

text/comma-separated-values

Label:

Rh6-6.csv

Text:

Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.03% strain amplitude (Fig. 5)

text/comma-separated-values

Label:

Rh6-7.csv

Text:

Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.2% strain amplitude (Fig. 5)

text/comma-separated-values

Label:

Rh6-8.csv

Text:

Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.2% strain amplitude (Fig. 5)

text/comma-separated-values

Label:

Rh6-9.csv

Text:

Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.2% strain amplitude (Fig. 5)

text/comma-separated-values

Label:

Rh7a-1.csv

Text:

Rotational shear rate sweep from 0.001 to 1000 1/s (Fig. 4a, 4b)

text/comma-separated-values

Label:

Rh7a-2.csv

Text:

Rotational shear rate sweep from 0.01 to 1 1/s (Fig. 4a, 4b)

text/comma-separated-values

Label:

Rh7a-3.csv

Text:

Rotational shear rate sweep from 0.001 to 0.01 1/s (Fig. 4a, 4b)

text/comma-separated-values

Label:

Rh7a-4.csv

Text:

Rotational shear rate sweep from 1 to 100 1/s (Fig. 4a, 4b)

text/comma-separated-values

Label:

Rh7a-5.csv

Text:

Rotational shear rate sweep from 10 to 1000 1/s (Fig. 4a, 4b)

text/comma-separated-values

Label:

Rh7b-1.csv

Text:

Rotational shear rate sweep from 0.1 to 100 1/s with sandpaper (Fig. 4a, 4b)

text/comma-separated-values

Label:

Rh7b-2.csv

Text:

Rotational shear rate sweep from 0.1 to 100 1/s with sandpaper (Fig. 4a, 4b)

text/comma-separated-values

Label:

Rh7b-3.csv

Text:

Rotational shear rate sweep from 0.1 to 100 1/s with sandpaper (Fig. 4a, 4b)

text/comma-separated-values

Label:

Rh8-1.csv

Text:

Constant rotational shear rate 0.0001 1/s for 20 minutes (Fig. 4c)

text/comma-separated-values

Label:

Rh8-2.csv

Text:

Constant rotational shear rate 0.001 1/s for 20 minutes (Fig. 4c)

text/comma-separated-values

Label:

Rh8-3.csv

Text:

Constant rotational shear rate 0.01 1/s for 20 minutes (Fig. 4c)

text/comma-separated-values

Label:

Rh8-4.csv

Text:

Constant rotational shear rate 0.1 1/s for 20 minutes (Fig. 4c)

text/comma-separated-values

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Rh8-5.csv

Text:

Constant rotational shear rate 1 1/s for 20 minutes (Fig. 4c)

text/comma-separated-values

Label:

Rh8-6.csv

Text:

Constant rotational shear rate 100 1/s for 20 minutes (Fig. 4c)

text/comma-separated-values

Label:

Rh9.csv

Text:

Bone cement was prepared and simply left on the rheometer between the plates while maintaining 1.5 mm gap for 45 minutes without any action

text/comma-separated-values

Label:

settings.xlsx

Text:

Contains settings for all the measurements

application/vnd.openxmlformats-officedocument.spreadsheetml.sheet